(Z)-1-(6-O-acetyl-2,3,4-tri-O-benzyl-α-D-glucopyranosyl)-2-phenylethylene

Base Information

• Chemical Name: (Z)-1-(6-O-acetyl-2,3,4-tri-O-benzyl-α-D-glucopyranosyl)-2-phenylethylene
• CAS No.: 164528-33-0
• Molecular Formula: C₃₇H₃₈O₆
• Molecular Weight: 578.705

Synonyms:(Z)-1-(6-O-acetyl-2,3,4-tri-O-benzyl-α-D-glucopyranosyl)-2-phenylethylene

Chemical Property of (Z)-1-(6-O-acetyl-2,3,4-tri-O-benzyl-α-D-glucopyranosyl)-2-phenylethylene

Chemical Property:

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Technology Process of (Z)-1-(6-O-acetyl-2,3,4-tri-O-benzyl-α-D-glucopyranosyl)-2-phenylethylene

There total 1 articles about (Z)-1-(6-O-acetyl-2,3,4-tri-O-benzyl-α-D-glucopyranosyl)-2-phenylethylene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

1-(6-O-acetyl-2,3,4-tri-O-benzyl-α-D-glucopyranosyl)-2-phenylacetylene → (Z)-1-(6-O-acetyl-2,3,4-tri-O-benzyl-α-D-glucopyranosyl)-2-phenylethylene (164528-33-0)

Guidance literature:

With acetic acid; zinc; In methanol; for 4h; Heating;

DOI:10.1016/0008-6215(94)00326-B

Reference yield: 90.0%

(Z)-1-(6-O-acetyl-2,3,4-tri-O-benzyl-α-D-glucopyranosyl)-2-phenylethylene (164528-33-0) → (Z)-1-(2,3,4-tri-O-benzyl-α-D-glucopyranosyl)-2-phenylethylene

Guidance literature:

With methanol; sodium methylate; Ambient temperature;

DOI:10.1016/0008-6215(94)00326-B

Reference yield:

(Z)-1-(6-O-acetyl-2,3,4-tri-O-benzyl-α-D-glucopyranosyl)-2-phenylethylene (164528-33-0) → 7-O-acetyl-2,6-anhydro-3,4,5-tri-O-benzyl-D-glycero-D-iso-heptose

Guidance literature:

With ozone; triphenylphosphine; Multistep reaction; 1.) CH₂Cl₂, -70 deg C, 2.) CH₂Cl₂, a) -70 deg C, 40 min, b) RT, 3 h;

DOI:10.1016/0008-6215(94)00326-B

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