7,4'-di-O-(1-O-methyl-2,3,4-tri-O-acetyl-6-deoxy-α-D-glicopyrane-6-yl)-genistein

Base Information

Chemical Name:7,4'-di-O-(1-O-methyl-2,3,4-tri-O-acetyl-6-deoxy-α-D-glicopyrane-6-yl)-genistein
CAS No.:1623075-86-4
Molecular Formula:C₂₈H₂₈O₁₃
Molecular Weight:572.523
Hs Code.:

Synonyms:7,4'-di-O-(1-O-methyl-2,3,4-tri-O-acetyl-6-deoxy-α-D-glicopyrane-6-yl)-genistein

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Chemical Property of 7,4'-di-O-(1-O-methyl-2,3,4-tri-O-acetyl-6-deoxy-α-D-glicopyrane-6-yl)-genistein

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Technology Process of 7,4'-di-O-(1-O-methyl-2,3,4-tri-O-acetyl-6-deoxy-α-D-glicopyrane-6-yl)-genistein

There total 3 articles about 7,4'-di-O-(1-O-methyl-2,3,4-tri-O-acetyl-6-deoxy-α-D-glicopyrane-6-yl)-genistein which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 446-72-0
5,7-Dihydroxy-3-(4-hydroxy-phenyl)-chromen-4-on

: 6304-96-7
methyl 2,3,4-tri-O-acetyl-6-deoxy-6-iodo-α-D-glucopyranoside

: 1623075-87-5
7-O-(1-O-methyl-2,3,4-tri-O-acetyl-6-deoxy-α-D-glicopyrane-6-yl)-genistein

: 1623075-86-4
7,4'-di-O-(1-O-methyl-2,3,4-tri-O-acetyl-6-deoxy-α-D-glicopyrane-6-yl)-genistein

Guidance literature:: 5,7-Dihydroxy-3-(4-hydroxy-phenyl)-chromen-4-on; With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 1h;

methyl 2,3,4-tri-O-acetyl-6-deoxy-6-iodo-α-D-glucopyranoside; In N,N-dimethyl-formamide; at 80 ℃; for 48h;
DOI:10.1016/j.ejmech.2014.08.032

Reference yield:

: 97-30-3
methyl-alpha-D-glucopyranoside

: 1623075-86-4
7,4'-di-O-(1-O-methyl-2,3,4-tri-O-acetyl-6-deoxy-α-D-glicopyrane-6-yl)-genistein

Guidance literature:: Multi-step reaction with 3 steps

1.1: iodine; triphenylphosphine; 1H-imidazole / toluene / 24 h / 80 °C

2.1: pyridine / 24 h / 0 - 20 °C

3.1: potassium carbonate / N,N-dimethyl-formamide / 1 h / 20 °C

3.2: 48 h / 80 °C

With pyridine; 1H-imidazole; iodine; potassium carbonate; triphenylphosphine; In N,N-dimethyl-formamide; toluene;
DOI:10.1016/j.ejmech.2014.08.032

Reference yield:

: 5155-46-4
methyl 6-iodo-6-deoxy-α-D-glucopyranoside

: 1623075-86-4
7,4'-di-O-(1-O-methyl-2,3,4-tri-O-acetyl-6-deoxy-α-D-glicopyrane-6-yl)-genistein

Guidance literature:: Multi-step reaction with 2 steps

1.1: pyridine / 24 h / 0 - 20 °C

2.1: potassium carbonate / N,N-dimethyl-formamide / 1 h / 20 °C

2.2: 48 h / 80 °C

With pyridine; potassium carbonate; In N,N-dimethyl-formamide;
DOI:10.1016/j.ejmech.2014.08.032