benzyl (R)-2-((1R,2R,5S)-3,6-dioxabicyclo[3.1.0]hexan-2-yl)propylcarbamate

Base Information

Chemical Name:benzyl (R)-2-((1R,2R,5S)-3,6-dioxabicyclo[3.1.0]hexan-2-yl)propylcarbamate
CAS No.:1172140-03-2
Molecular Formula:C₁₅H₁₉NO₄
Molecular Weight:277.32
Hs Code.:

Synonyms:benzyl (R)-2-((1R,2R,5S)-3,6-dioxabicyclo[3.1.0]hexan-2-yl)propylcarbamate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of benzyl (R)-2-((1R,2R,5S)-3,6-dioxabicyclo[3.1.0]hexan-2-yl)propylcarbamate

Chemical Property:

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Technology Process of benzyl (R)-2-((1R,2R,5S)-3,6-dioxabicyclo[3.1.0]hexan-2-yl)propylcarbamate

There total 8 articles about benzyl (R)-2-((1R,2R,5S)-3,6-dioxabicyclo[3.1.0]hexan-2-yl)propylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1172140-02-1
benzyl (R)-2-((S)-2,5-dihydrofuran-2-yl)-2-hydroxyethyl carbamate

: 1172140-03-2
benzyl (R)-2-((1R,2R,5S)-3,6-dioxabicyclo[3.1.0]hexan-2-yl)propylcarbamate

: 1308300-07-3
C₁₅H₁₉NO₄

Guidance literature:: With Oxone; 1,1,1-trifluoro-2-propanone; sodium hydrogencarbonate; In water; acetonitrile; at 0 ℃; for 1.66667h;

Reference yield:

: 1172140-02-1
benzyl (R)-2-((S)-2,5-dihydrofuran-2-yl)-2-hydroxyethyl carbamate

: 1172140-03-2
benzyl (R)-2-((1R,2R,5S)-3,6-dioxabicyclo[3.1.0]hexan-2-yl)propylcarbamate

: C₁₅H₁₉NO₄

: 1308300-07-3
C₁₅H₁₉NO₄

Guidance literature:: With Oxone; 1,1,1-trifluoro-2-propanone; edetate disodium; sodium hydrogencarbonate; In water; acetonitrile; at 0 ℃; for 1.66667h;

Reference yield:

: 1172140-01-0
(R)-2-((S)-2,5-dihydrofuran-2-yl)propyl methanesulfonate

: 1172140-03-2
benzyl (R)-2-((1R,2R,5S)-3,6-dioxabicyclo[3.1.0]hexan-2-yl)propylcarbamate

: 1308300-07-3
C₁₅H₁₉NO₄

Guidance literature:: Multi-step reaction with 3 steps

1: ammonium hydroxide; ammonia; water / isopropyl alcohol / 20 h / 20 - 70 °C

2: sodium carbonate / 1,4-dioxane; water / 0.83 h

3: Oxone; 1,1,1-trifluoro-2-propanone; sodium hydrogencarbonate / water; acetonitrile / 1.67 h / 0 °C

With Oxone; ammonium hydroxide; 1,1,1-trifluoro-2-propanone; ammonia; water; sodium hydrogencarbonate; sodium carbonate; In 1,4-dioxane; water; isopropyl alcohol; acetonitrile;