3-(tert-butyldimethylsilyl)-2,3-dihydroxy-1-tosylpropyl diisopropylcarbamate

Base Information

Chemical Name:3-(tert-butyldimethylsilyl)-2,3-dihydroxy-1-tosylpropyl diisopropylcarbamate
CAS No.:1443780-15-1
Molecular Formula:C₂₃H₄₁NO₆SSi
Molecular Weight:487.733
Hs Code.:

Synonyms:3-(tert-butyldimethylsilyl)-2,3-dihydroxy-1-tosylpropyl diisopropylcarbamate

Suppliers and Price of 3-(tert-butyldimethylsilyl)-2,3-dihydroxy-1-tosylpropyl diisopropylcarbamate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of 3-(tert-butyldimethylsilyl)-2,3-dihydroxy-1-tosylpropyl diisopropylcarbamate

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

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Technology Process of 3-(tert-butyldimethylsilyl)-2,3-dihydroxy-1-tosylpropyl diisopropylcarbamate

There total 4 articles about 3-(tert-butyldimethylsilyl)-2,3-dihydroxy-1-tosylpropyl diisopropylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 1443780-14-0
(E)-3-(tert-butyldimethylsilyl)-1-tosylallyl diisopropylcarbamate

: 1443780-15-1
3-(tert-butyldimethylsilyl)-2,3-dihydroxy-1-tosylpropyl diisopropylcarbamate

Guidance literature:: With osmium(VIII) oxide; 4-methylmorpholine N-oxide; In water; acetone; acetonitrile; at 20 ℃; for 1.33333h;
DOI:10.1016/j.tet.2013.05.043

Reference yield:

: 1443780-03-7
(E)-3-(tert-butyldimethylsilyl)allyl diisopropylcarbamate

: 1443780-15-1
3-(tert-butyldimethylsilyl)-2,3-dihydroxy-1-tosylpropyl diisopropylcarbamate

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-butyllithium; N,N,N,N,-tetramethylethylenediamine / hexane; tetrahydrofuran / 0.17 h / -80 °C

1.2: 0.17 h / -80 °C

2.1: osmium(VIII) oxide; 4-methylmorpholine N-oxide / acetonitrile; acetone; water / 1.33 h / 20 °C

With osmium(VIII) oxide; n-butyllithium; N,N,N,N,-tetramethylethylenediamine; 4-methylmorpholine N-oxide; In tetrahydrofuran; hexane; water; acetone; acetonitrile;
DOI:10.1016/j.tet.2013.05.043

Reference yield:

: 19009-39-3
N,N-diisopropylcarbamoyl chloride

: 1443780-15-1
3-(tert-butyldimethylsilyl)-2,3-dihydroxy-1-tosylpropyl diisopropylcarbamate

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium hexamethylsilazane / tetrahydrofuran / 0.17 h / -80 °C

1.2: 0.42 h / -80 - 0 °C

2.1: n-butyllithium; N,N,N,N,-tetramethylethylenediamine / hexane; tetrahydrofuran / 0.17 h / -80 °C

2.2: 0.17 h / -80 °C

3.1: osmium(VIII) oxide; 4-methylmorpholine N-oxide / acetonitrile; acetone; water / 1.33 h / 20 °C

With osmium(VIII) oxide; n-butyllithium; N,N,N,N,-tetramethylethylenediamine; potassium hexamethylsilazane; 4-methylmorpholine N-oxide; In tetrahydrofuran; hexane; water; acetone; acetonitrile;
DOI:10.1016/j.tet.2013.05.043