8,9-difluoro-5-methoxy-5-[4-(2-piperidin-1-yl-ethoxy)-phenyl]-5H-6-oxa-chrysen-2-ol

Base Information

Chemical Name:8,9-difluoro-5-methoxy-5-[4-(2-piperidin-1-yl-ethoxy)-phenyl]-5H-6-oxa-chrysen-2-ol
CAS No.:861931-84-2
Molecular Formula:C₃₁H₂₉F₂NO₄
Molecular Weight:517.572
Hs Code.:

Synonyms:8,9-difluoro-5-methoxy-5-[4-(2-piperidin-1-yl-ethoxy)-phenyl]-5H-6-oxa-chrysen-2-ol

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Chemical Property of 8,9-difluoro-5-methoxy-5-[4-(2-piperidin-1-yl-ethoxy)-phenyl]-5H-6-oxa-chrysen-2-ol

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Technology Process of 8,9-difluoro-5-methoxy-5-[4-(2-piperidin-1-yl-ethoxy)-phenyl]-5H-6-oxa-chrysen-2-ol

There total 1 articles about 8,9-difluoro-5-methoxy-5-[4-(2-piperidin-1-yl-ethoxy)-phenyl]-5H-6-oxa-chrysen-2-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 861931-83-1
[2-(4,5-difluoro-2-methoxy-phenyl)-6-methoxy-naphthalen-1-yl]-[4-(2-piperidin-1-yl-ethoxy)-phenyl]-methanone

: 861931-84-2
8,9-difluoro-5-methoxy-5-[4-(2-piperidin-1-yl-ethoxy)-phenyl]-5H-6-oxa-chrysen-2-ol

Guidance literature:: [2-(4,5-difluoro-2-methoxy-phenyl)-6-methoxy-naphthalen-1-yl]-[4-(2-piperidin-1-yl-ethoxy)-phenyl]-methanone; With hydrogenchloride; In water;

With boron tribromide; In dichloromethane; at 0 - 20 ℃; for 1h;

With methanol; In dichloromethane;

Reference yield: 18.0%

: 861931-84-2
8,9-difluoro-5-methoxy-5-[4-(2-piperidin-1-yl-ethoxy)-phenyl]-5H-6-oxa-chrysen-2-ol

: 861931-85-3
8,9-difluoro-5-[4-(2-piperidin-1-yl-ethoxy)-phenyl]-5H-6-oxa-chrysen-2-ol

Guidance literature:: With triethylamine; trifluoroacetic acid; In dichloromethane; at 20 ℃; for 1h;

Reference yield:

: 861931-84-2
8,9-difluoro-5-methoxy-5-[4-(2-piperidin-1-yl-ethoxy)-phenyl]-5H-6-oxa-chrysen-2-ol

: 5-[4-(2-diethylamino-ethoxy)-phenyl]-8,9-difluoro-5H-6-oxa-chrysen-2-ol

Guidance literature:: 8,9-difluoro-5-methoxy-5-[4-(2-piperidin-1-yl-ethoxy)-phenyl]-5H-6-oxa-chrysen-2-ol; With triethylsilane; trifluoroacetic acid; In chloroform; at 0 - 20 ℃; for 4h; Heating / reflux;

With sodium hydroxide; In chloroform; water;