C₃₆H₅₁NO₃Si

Base Information

Chemical Name:C₃₆H₅₁NO₃Si
CAS No.:1374425-40-7
Molecular Formula:C₃₆H₅₁NO₃Si
Molecular Weight:573.891
Hs Code.:

C<sub>36</sub>H<sub>51</sub>NO<sub>3</sub>Si

Synonyms:C₃₆H₅₁NO₃Si

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Chemical Property of C₃₆H₅₁NO₃Si

Chemical Property:

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Technology Process of C₃₆H₅₁NO₃Si

There total 19 articles about C₃₆H₅₁NO₃Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 37.0%

: 18871-66-4
N,N-dimethylacetamide dimethyl acetal

: 1374425-33-8
C₃₂H₄₄O₃Si

: 1374425-36-1
C₃₃H₄₃NO₃

: 1374425-40-7
C₃₆H₅₁NO₃Si

Guidance literature:: In 1,2-dichloro-benzene; at 220 ℃; for 1h; Microwave irradiation; Inert atmosphere;
DOI:10.1002/ejoc.201101629

Reference yield:

: C₁₆H₂₈O₃Si

: 1374425-40-7
C₃₆H₅₁NO₃Si

Guidance literature:: Multi-step reaction with 14 steps

1.1: ozone / dichloromethane / 3 h / -78 °C

1.2: 4 h / 20 °C / Inert atmosphere

2.1: methanol; diethyl ether; toluene / 0.25 h / Inert atmosphere

3.1: lithium aluminium tetrahydride / tetrahydrofuran; dichloromethane / 0.5 h / 0 °C / Inert atmosphere

4.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.5 h / 0 °C / Inert atmosphere

4.2: 16 h / 20 °C / Inert atmosphere

5.1: toluene-4-sulfonic acid / water; acetone / 0.5 h / 20 °C

6.1: triethylamine / dichloromethane / 0.75 h / 0 °C / Inert atmosphere

7.1: oxygen; palladium diacetate / dimethyl sulfoxide / 16 h / 20 - 80 °C

8.1: iodine; magnesium / tetrahydrofuran / 2 h / 70 °C / Inert atmosphere

8.2: 0.5 h / -78 °C / Inert atmosphere

8.3: 5 h / -78 °C / Inert atmosphere

9.1: toluene-4-sulfonic acid / acetone / 0.5 h / 20 °C / Inert atmosphere

10.1: n-butyllithium; lithium diisopropyl amide / tetrahydrofuran; cyclohexane / 1 h / -78 °C / Inert atmosphere

10.2: 3 h / -78 °C / Inert atmosphere

11.1: pyridine; dihydrogen peroxide / dichloromethane; water / 0.5 h / 0 - 20 °C

12.1: diisobutylaluminium hydride / dichloromethane; toluene / 0.25 h / -78 °C / Inert atmosphere

13.1: 1,2-dichloro-benzene / 1 h / 220 °C / Microwave irradiation; Inert atmosphere

14.1: lithium diisopropyl amide / tetrahydrofuran / 1 h / -78 °C / Inert atmosphere

14.2: 0.5 h / -78 - 20 °C / Inert atmosphere

With pyridine; lithium aluminium tetrahydride; n-butyllithium; dihydrogen peroxide; iodine; oxygen; palladium diacetate; sodium hydride; diisobutylaluminium hydride; toluene-4-sulfonic acid; ozone; magnesium; triethylamine; lithium diisopropyl amide; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; cyclohexane; water; dimethyl sulfoxide; N,N-dimethyl-formamide; 1,2-dichloro-benzene; acetone; toluene; mineral oil;
DOI:10.1002/ejoc.201101629

Reference yield:

: 1374425-20-3
C₁₃H₂₀O₃

: 1374425-40-7
C₃₆H₅₁NO₃Si

Guidance literature:: Multi-step reaction with 15 steps

1.1: triethylamine / dichloromethane / 3 h / -78 °C / Inert atmosphere

2.1: ozone / dichloromethane / 3 h / -78 °C

2.2: 4 h / 20 °C / Inert atmosphere

3.1: methanol; diethyl ether; toluene / 0.25 h / Inert atmosphere

4.1: lithium aluminium tetrahydride / tetrahydrofuran; dichloromethane / 0.5 h / 0 °C / Inert atmosphere

5.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.5 h / 0 °C / Inert atmosphere

5.2: 16 h / 20 °C / Inert atmosphere

6.1: toluene-4-sulfonic acid / water; acetone / 0.5 h / 20 °C

7.1: triethylamine / dichloromethane / 0.75 h / 0 °C / Inert atmosphere

8.1: oxygen; palladium diacetate / dimethyl sulfoxide / 16 h / 20 - 80 °C

9.1: iodine; magnesium / tetrahydrofuran / 2 h / 70 °C / Inert atmosphere

9.2: 0.5 h / -78 °C / Inert atmosphere

9.3: 5 h / -78 °C / Inert atmosphere

10.1: toluene-4-sulfonic acid / acetone / 0.5 h / 20 °C / Inert atmosphere

11.1: n-butyllithium; lithium diisopropyl amide / tetrahydrofuran; cyclohexane / 1 h / -78 °C / Inert atmosphere

11.2: 3 h / -78 °C / Inert atmosphere

12.1: pyridine; dihydrogen peroxide / dichloromethane; water / 0.5 h / 0 - 20 °C

13.1: diisobutylaluminium hydride / dichloromethane; toluene / 0.25 h / -78 °C / Inert atmosphere

14.1: 1,2-dichloro-benzene / 1 h / 220 °C / Microwave irradiation; Inert atmosphere

15.1: lithium diisopropyl amide / tetrahydrofuran / 1 h / -78 °C / Inert atmosphere

15.2: 0.5 h / -78 - 20 °C / Inert atmosphere

With pyridine; lithium aluminium tetrahydride; n-butyllithium; dihydrogen peroxide; iodine; oxygen; palladium diacetate; sodium hydride; diisobutylaluminium hydride; toluene-4-sulfonic acid; ozone; magnesium; triethylamine; lithium diisopropyl amide; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; cyclohexane; water; dimethyl sulfoxide; N,N-dimethyl-formamide; 1,2-dichloro-benzene; acetone; toluene; mineral oil;
DOI:10.1002/ejoc.201101629