2-benzyloxycarbonylmethylthio-3-cyano-4-ethyl-5,6-hexamethylenepyridine

Base Information

• Chemical Name: 2-benzyloxycarbonylmethylthio-3-cyano-4-ethyl-5,6-hexamethylenepyridine
• CAS No.: 380217-77-6
• Molecular Formula: C₂₃H₂₆N₂O₂S
• Molecular Weight: 394.538

Synonyms:2-benzyloxycarbonylmethylthio-3-cyano-4-ethyl-5,6-hexamethylenepyridine

Chemical Property of 2-benzyloxycarbonylmethylthio-3-cyano-4-ethyl-5,6-hexamethylenepyridine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-benzyloxycarbonylmethylthio-3-cyano-4-ethyl-5,6-hexamethylenepyridine

There total 2 articles about 2-benzyloxycarbonylmethylthio-3-cyano-4-ethyl-5,6-hexamethylenepyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

3-cyano-4-ethyl-5,6-hexamethylenepyridine-2(1H)-thione (381189-58-8) + Benzyl chloroacetate (140-18-1) → 2-benzyloxycarbonylmethylthio-3-cyano-4-ethyl-5,6-hexamethylenepyridine (380217-77-6)

Guidance literature:

With potassium hydroxide; In N,N-dimethyl-formamide; for 4h;

DOI:10.1007/s10593-005-0244-y

Reference yield:

1-(morpholin-4-yl)cyclooctene (101471-72-1) → 2-benzyloxycarbonylmethylthio-3-cyano-4-ethyl-5,6-hexamethylenepyridine (380217-77-6)

Guidance literature:

Multi-step reaction with 2 steps

1: 75 percent / ethanol / 25 h / 20 °C

2: 72 percent / aq. KOH / dimethylformamide / 4 h

With potassium hydroxide; In ethanol; N,N-dimethyl-formamide;

DOI:10.1007/s10593-005-0244-y

Reference yield: 89.0%

2-benzyloxycarbonylmethylthio-3-cyano-4-ethyl-5,6-hexamethylenepyridine (380217-77-6) → 3-amino-2-benzyloxycarbonyl-4-ethyl-5,6-hexamethylenethieno[2,3-b]pyridine

Guidance literature:

With potassium hydroxide; In N,N-dimethyl-formamide; for 5h;

DOI:10.1007/s10593-005-0244-y

upstream raw materials:

3-cyano-4-ethyl-5,6-hexamethylenepyridine-2(1H)-thione

Benzyl chloroacetate

1-(morpholin-4-yl)cyclooctene

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 380217-77-6 2-benzyloxycarbonylmethylthio-3-cyano-4-ethyl-5,6-hexamethylenepyridine

Send

Send

Metric Ton KG G Pound L ML

Send

Send