Technology Process of N~2~,N~7~-diphenyl-9H-fluorene-2,7-disulfonamide
There total 3 articles about N~2~,N~7~-diphenyl-9H-fluorene-2,7-disulfonamide which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium hydroxide;
In
tetrahydrofuran; water; acetone;
at 100 ℃;
for 0.25h;
Microwave irradiation;
DOI:10.1055/s-0036-1588916
- Guidance literature:
-
Multi-step reaction with 2 steps
1: phosphorus pentachloride; trichlorophosphate / 16 h / Reflux
2: sodium hydroxide / acetone; tetrahydrofuran; water / 0.25 h / 100 °C / Microwave irradiation
With
phosphorus pentachloride; sodium hydroxide; trichlorophosphate;
In
tetrahydrofuran; water; acetone;
DOI:10.1055/s-0036-1588916
- Guidance literature:
-
Multi-step reaction with 3 steps
1: acetic acid; chlorosulfonic acid / 16 h / 0 - 140 °C
2: phosphorus pentachloride; trichlorophosphate / 16 h / Reflux
3: sodium hydroxide / acetone; tetrahydrofuran; water / 0.25 h / 100 °C / Microwave irradiation
With
chlorosulfonic acid; phosphorus pentachloride; acetic acid; sodium hydroxide; trichlorophosphate;
In
tetrahydrofuran; water; acetone;
DOI:10.1055/s-0036-1588916
