2-(4-((2-(3-chlorophenyl)-6-cyclopropylpyridin-4-yl)amino)phenyl)acetamide hydrochloride

Base Information

Chemical Name:2-(4-((2-(3-chlorophenyl)-6-cyclopropylpyridin-4-yl)amino)phenyl)acetamide hydrochloride
CAS No.:1606974-30-4
Molecular Formula:C₂₂H₂₀ClN₃O*ClH
Molecular Weight:414.334
Hs Code.:

Synonyms:2-(4-((2-(3-chlorophenyl)-6-cyclopropylpyridin-4-yl)amino)phenyl)acetamide hydrochloride

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Chemical Property of 2-(4-((2-(3-chlorophenyl)-6-cyclopropylpyridin-4-yl)amino)phenyl)acetamide hydrochloride

Chemical Property:

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Technology Process of 2-(4-((2-(3-chlorophenyl)-6-cyclopropylpyridin-4-yl)amino)phenyl)acetamide hydrochloride

There total 5 articles about 2-(4-((2-(3-chlorophenyl)-6-cyclopropylpyridin-4-yl)amino)phenyl)acetamide hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 1606976-99-1
2-(4-((2-(3-chlorophenyl)-6-cyclopropylpyridin-4-yl)amino)phenyl)acetamide

: 1606974-30-4
2-(4-((2-(3-chlorophenyl)-6-cyclopropylpyridin-4-yl)amino)phenyl)acetamide hydrochloride

Guidance literature:: With hydrogenchloride; In methanol;

Reference yield:

: 1606976-97-9
4-chloro-2-(3-chlorophenyl)-6-cyclopropylpyridine

: 1606974-30-4
2-(4-((2-(3-chlorophenyl)-6-cyclopropylpyridin-4-yl)amino)phenyl)acetamide hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1: caesium carbonate; palladium diacetate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl / 1,4-dioxane / 2 h / 120 °C / Microwave irradiation; Inert atmosphere

2: ammonia / 1,4-dioxane; methanol / 47 h / 100 °C / Sealed tube

3: hydrogenchloride / methanol

With hydrogenchloride; ammonia; palladium diacetate; caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; In 1,4-dioxane; methanol;

Reference yield:

: 16063-69-7
2,4,6-trichloropyridine

: 1606974-30-4
2-(4-((2-(3-chlorophenyl)-6-cyclopropylpyridin-4-yl)amino)phenyl)acetamide hydrochloride

Guidance literature:: Multi-step reaction with 5 steps

1: palladium diacetate; tricyclohexylphosphine; potassium phosphate / toluene; water / 24 h / 90 °C / Inert atmosphere

2: caesium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene; ethanol; water / 23 h / 90 °C / Inert atmosphere

3: caesium carbonate; palladium diacetate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl / 1,4-dioxane / 2 h / 120 °C / Microwave irradiation; Inert atmosphere

4: ammonia / 1,4-dioxane; methanol / 47 h / 100 °C / Sealed tube

5: hydrogenchloride / methanol

With hydrogenchloride; potassium phosphate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; ammonia; palladium diacetate; caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; tricyclohexylphosphine; In 1,4-dioxane; methanol; ethanol; water; toluene;