C₂₂H₂₃IO₅

Base Information

Chemical Name:C₂₂H₂₃IO₅
CAS No.:1311379-31-3
Molecular Formula:C₂₂H₂₃IO₅
Molecular Weight:494.326
Hs Code.:

C<sub>22</sub>H<sub>23</sub>IO<sub>5</sub>

Synonyms:C₂₂H₂₃IO₅

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Chemical Property of C₂₂H₂₃IO₅

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Technology Process of C₂₂H₂₃IO₅

There total 10 articles about C₂₂H₂₃IO₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 1311379-24-4
C₂₂H₂₂O₅

: 1311379-31-3
C₂₂H₂₃IO₅

: 1311379-29-9
C₂₂H₂₃IO₅

Guidance literature:: With magnesium iodide; In dichloromethane; at -78 - -20 ℃; diastereoselective reaction; Inert atmosphere;
DOI:10.1021/ja203642n

Reference yield:

: C₁₇H₂₀O₄

: 1311379-31-3
C₂₂H₂₃IO₅

: 1311379-29-9
C₂₂H₂₃IO₅

Guidance literature:: Multi-step reaction with 6 steps

1: sodium chlorite; sodium phosphate monobasic monohydrate / 2-methyl-but-2-ene; water; tert-butyl alcohol / 0 °C

2: sulfuric acid / 0 - 20 °C / Inert atmosphere

3: toluene-4-sulfonic acid / tetrahydrofuran / 80 °C / Inert atmosphere

4: chloro-trimethyl-silane; sodium cyanoborohydride / acetonitrile / 0 °C / Inert atmosphere; Heating

5: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / ethyl acetate / 3 h / 80 °C / Inert atmosphere

6: magnesium iodide / dichloromethane / -78 - -20 °C / Inert atmosphere

With sodium chlorite; chloro-trimethyl-silane; sodium phosphate monobasic monohydrate; sulfuric acid; sodium cyanoborohydride; toluene-4-sulfonic acid; magnesium iodide; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In tetrahydrofuran; 2-methyl-but-2-ene; dichloromethane; water; ethyl acetate; acetonitrile; tert-butyl alcohol; 1: Pinnick oxidation / 6: intramolecular halo-Michael aldol reaction;
DOI:10.1021/ja203642n

Reference yield:

: C₁₇H₂₀O₅

: 1311379-31-3
C₂₂H₂₃IO₅

: 1311379-29-9
C₂₂H₂₃IO₅

Guidance literature:: Multi-step reaction with 5 steps

1: sulfuric acid / 0 - 20 °C / Inert atmosphere

2: toluene-4-sulfonic acid / tetrahydrofuran / 80 °C / Inert atmosphere

3: chloro-trimethyl-silane; sodium cyanoborohydride / acetonitrile / 0 °C / Inert atmosphere; Heating

4: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / ethyl acetate / 3 h / 80 °C / Inert atmosphere

5: magnesium iodide / dichloromethane / -78 - -20 °C / Inert atmosphere

With chloro-trimethyl-silane; sulfuric acid; sodium cyanoborohydride; toluene-4-sulfonic acid; magnesium iodide; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In tetrahydrofuran; dichloromethane; ethyl acetate; acetonitrile; 5: intramolecular halo-Michael aldol reaction;
DOI:10.1021/ja203642n