methyl-phenyl-carbamic acid 6-[(methyl-pyridin-2-ylmethyl-amino)-methyl]-pyridin-2-yl ester

Base Information

Chemical Name:methyl-phenyl-carbamic acid 6-[(methyl-pyridin-2-ylmethyl-amino)-methyl]-pyridin-2-yl ester
CAS No.:386265-30-1
Molecular Formula:C₂₁H₂₂N₄O₂
Molecular Weight:362.431
Hs Code.:

Synonyms:methyl-phenyl-carbamic acid 6-[(methyl-pyridin-2-ylmethyl-amino)-methyl]-pyridin-2-yl ester

Suppliers and Price of methyl-phenyl-carbamic acid 6-[(methyl-pyridin-2-ylmethyl-amino)-methyl]-pyridin-2-yl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of methyl-phenyl-carbamic acid 6-[(methyl-pyridin-2-ylmethyl-amino)-methyl]-pyridin-2-yl ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of methyl-phenyl-carbamic acid 6-[(methyl-pyridin-2-ylmethyl-amino)-methyl]-pyridin-2-yl ester

There total 3 articles about methyl-phenyl-carbamic acid 6-[(methyl-pyridin-2-ylmethyl-amino)-methyl]-pyridin-2-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 4285-42-1
N-phenyl-N-methylcarbamoyl chloride

: 386265-28-7
6-[(methyl-pyridin-2-ylmethyl-amino)-methyl]-1H-pyridin-2-one

: 386265-30-1
methyl-phenyl-carbamic acid 6-[(methyl-pyridin-2-ylmethyl-amino)-methyl]-pyridin-2-yl ester

Guidance literature:: With triethylamine; In acetonitrile; Heating;
DOI:10.1021/ol016867z

Reference yield:

: 2683-51-4
2-acetoxy-6-methylpyridine

: 386265-30-1
methyl-phenyl-carbamic acid 6-[(methyl-pyridin-2-ylmethyl-amino)-methyl]-pyridin-2-yl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 52 percent / 2,2'-azobisisobutyronitrile; N-bromosuccinimide / CCl₄ / Heating

2: 49 percent / triethylamine / CH₂Cl₂ / 2 h / 20 °C

3: 87 percent / triethylamine / acetonitrile / Heating

With N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); triethylamine; In tetrachloromethane; dichloromethane; acetonitrile;
DOI:10.1021/ol016867z

Reference yield:

: 386265-26-5
2-acetoxy-6-(bromomethyl)pyridine

: 386265-30-1
methyl-phenyl-carbamic acid 6-[(methyl-pyridin-2-ylmethyl-amino)-methyl]-pyridin-2-yl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 49 percent / triethylamine / CH₂Cl₂ / 2 h / 20 °C

2: 87 percent / triethylamine / acetonitrile / Heating

With triethylamine; In dichloromethane; acetonitrile;
DOI:10.1021/ol016867z