(2S,3R)-3-(-3-{(R)-1-[(S)-amino(benzyloxycarbonylmethylcarbamoyl)methyl]-1-methylprop-2-ynyloxy}-4-benzyloxyphenyl)-2-(benzyloxycarbonylmethylamino)-3-(tert-butyldimethylsilanyloxy)propionic acid 4-methoxybenzyl ester

Base Information

Chemical Name:(2S,3R)-3-(-3-{(R)-1-[(S)-amino(benzyloxycarbonylmethylcarbamoyl)methyl]-1-methylprop-2-ynyloxy}-4-benzyloxyphenyl)-2-(benzyloxycarbonylmethylamino)-3-(tert-butyldimethylsilanyloxy)propionic acid 4-methoxybenzyl ester
CAS No.:1013210-34-8
Molecular Formula:C₅₄H₆₃N₃O₁₁Si
Molecular Weight:958.193
Hs Code.:

(2S,3R)-3-(-3-{(R)-1-[(S)-amino(benzyloxycarbonylmethylcarbamoyl)methyl]-1-methylprop-2-ynyloxy}-4-benzyloxyphenyl)-2-(benzyloxycarbonylmethylamino)-3-(tert-butyldimethylsilanyloxy)propionic acid 4-methoxybenzyl ester

Synonyms:(2S,3R)-3-(-3-{(R)-1-[(S)-amino(benzyloxycarbonylmethylcarbamoyl)methyl]-1-methylprop-2-ynyloxy}-4-benzyloxyphenyl)-2-(benzyloxycarbonylmethylamino)-3-(tert-butyldimethylsilanyloxy)propionic acid 4-methoxybenzyl ester

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Chemical Property of (2S,3R)-3-(-3-{(R)-1-[(S)-amino(benzyloxycarbonylmethylcarbamoyl)methyl]-1-methylprop-2-ynyloxy}-4-benzyloxyphenyl)-2-(benzyloxycarbonylmethylamino)-3-(tert-butyldimethylsilanyloxy)propionic acid 4-methoxybenzyl ester

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Technology Process of (2S,3R)-3-(-3-{(R)-1-[(S)-amino(benzyloxycarbonylmethylcarbamoyl)methyl]-1-methylprop-2-ynyloxy}-4-benzyloxyphenyl)-2-(benzyloxycarbonylmethylamino)-3-(tert-butyldimethylsilanyloxy)propionic acid 4-methoxybenzyl ester

There total 1 articles about (2S,3R)-3-(-3-{(R)-1-[(S)-amino(benzyloxycarbonylmethylcarbamoyl)methyl]-1-methylprop-2-ynyloxy}-4-benzyloxyphenyl)-2-(benzyloxycarbonylmethylamino)-3-(tert-butyldimethylsilanyloxy)propionic acid 4-methoxybenzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 1013210-33-7
(2S,3R)-3-(4-benzyloxy-3-{(R)-1-[(S)-(benzyloxycarbonylmethylcarbamoyl)-(2-nitrobenzenesulfonylamino)methyl]-1-methylprop-2-ynyloxy}phenyl)-2-(benzyloxycarbonylmethylamino)-3-(tert-butyldimethylsilanyloxy)propionic acid 4-methoxybenzyl ester

: 1013210-34-8
(2S,3R)-3-(-3-{(R)-1-[(S)-amino(benzyloxycarbonylmethylcarbamoyl)methyl]-1-methylprop-2-ynyloxy}-4-benzyloxyphenyl)-2-(benzyloxycarbonylmethylamino)-3-(tert-butyldimethylsilanyloxy)propionic acid 4-methoxybenzyl ester

Guidance literature:: With caesium carbonate; thiophenol; In N,N-dimethyl-formamide; at 20 ℃; for 6h;
DOI:10.1021/ja710363p

Reference yield: 100.0%

: 1013210-34-8
(2S,3R)-3-(-3-{(R)-1-[(S)-amino(benzyloxycarbonylmethylcarbamoyl)methyl]-1-methylprop-2-ynyloxy}-4-benzyloxyphenyl)-2-(benzyloxycarbonylmethylamino)-3-(tert-butyldimethylsilanyloxy)propionic acid 4-methoxybenzyl ester

: 13139-16-7
N-(tert-butyloxycarbonyl)-L-isoleucine

: 1013210-60-0
C₆₅H₈₂N₄O₁₄Si

Guidance literature:: With sodium hydrogencarbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In N,N-dimethyl-formamide; at 20 ℃;
DOI:10.1021/ja710363p

Reference yield: 90.0%

: 1013210-34-8
(2S,3R)-3-(-3-{(R)-1-[(S)-amino(benzyloxycarbonylmethylcarbamoyl)methyl]-1-methylprop-2-ynyloxy}-4-benzyloxyphenyl)-2-(benzyloxycarbonylmethylamino)-3-(tert-butyldimethylsilanyloxy)propionic acid 4-methoxybenzyl ester

: 15761-38-3
L-N-Boc-Ala

: 1013210-57-5
C₆₂H₇₆N₄O₁₄Si

Guidance literature:: With sodium hydrogencarbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In N,N-dimethyl-formamide; at 20 ℃;
DOI:10.1021/ja710363p