diethyl benzyl-4-{bis[4-(diethoxyphosphorylmethyl)phenyl]methyl}phosphonate

Base Information

Chemical Name:diethyl benzyl-4-{bis[4-(diethoxyphosphorylmethyl)phenyl]methyl}phosphonate
CAS No.:340741-55-1
Molecular Formula:C₃₄H₄₉O₉P₃
Molecular Weight:694.679
Hs Code.:

Synonyms:diethyl benzyl-4-{bis[4-(diethoxyphosphorylmethyl)phenyl]methyl}phosphonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of diethyl benzyl-4-{bis[4-(diethoxyphosphorylmethyl)phenyl]methyl}phosphonate

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Technology Process of diethyl benzyl-4-{bis[4-(diethoxyphosphorylmethyl)phenyl]methyl}phosphonate

There total 2 articles about diethyl benzyl-4-{bis[4-(diethoxyphosphorylmethyl)phenyl]methyl}phosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 16845-02-6
tri-p-tolylmethane

: 122-52-1
triethyl phosphite

: 340741-55-1
diethyl benzyl-4-{bis[4-(diethoxyphosphorylmethyl)phenyl]methyl}phosphonate

Guidance literature:: at 150 ℃; for 8h;
DOI:10.1002/1099-0690(200103)2001:6<1163::aid-ejoc1163>3.0.co;2-k

Reference yield:

: 971-93-7
tri-p-tolylmethylchloride

: 340741-55-1
diethyl benzyl-4-{bis[4-(diethoxyphosphorylmethyl)phenyl]methyl}phosphonate

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / EtOH / 48 h / Heating

2: 65 percent / 8 h / 150 °C

With ethanol; 2: Arbuzov rearrangement;
DOI:10.1002/1099-0690(200103)2001:6<1163::aid-ejoc1163>3.0.co;2-k