C₁₅H₂₀O₄

Base Information

• Chemical Name: C₁₅H₂₀O₄
• CAS No.: 1474039-97-8
• Molecular Formula: C₁₅H₂₀O₄
• Molecular Weight: 264.321
• Mol file: 1474039-97-8.mol

Synonyms:C₁₅H₂₀O₄

Chemical Property of C₁₅H₂₀O₄

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₅H₂₀O₄

There total 3 articles about C₁₅H₂₀O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

C17H22O5 (131310-55-9) → C15H20O4 (1474039-97-8)

Guidance literature:

With diisobutylaluminium hydride; In dichloromethane; toluene; at -64 - -50 ℃; for 1.25h; Inert atmosphere;

DOI:10.1055/s-0033-1338503

Reference yield:

2-deoxy-D-ribose (22900-10-3,35536-75-5,36792-85-5,113890-34-9,113890-37-2,133813-23-7) → C15H20O4 (1474039-97-8)

Guidance literature:

Multi-step reaction with 3 steps

1: 2 h / Reflux; Inert atmosphere

2: trimethyl orthoformate; 10-camphorsufonic acid / dichloromethane / 22 h / 20 °C / Inert atmosphere

3: diisobutylaluminium hydride / dichloromethane; toluene / 1.25 h / -64 - -50 °C / Inert atmosphere

With 10-camphorsufonic acid; diisobutylaluminium hydride; trimethyl orthoformate; In dichloromethane; toluene; 1: |Wittig Olefination;

DOI:10.1055/s-0033-1338503

Reference yield:

(E)-(5S,6R)-5,6,7-Trihydroxy-2-methyl-hept-2-enoic acid ethyl ester (131310-54-8) → C15H20O4 (1474039-97-8)

Guidance literature:

Multi-step reaction with 2 steps

1: trimethyl orthoformate; 10-camphorsufonic acid / dichloromethane / 22 h / 20 °C / Inert atmosphere

2: diisobutylaluminium hydride / dichloromethane; toluene / 1.25 h / -64 - -50 °C / Inert atmosphere

With 10-camphorsufonic acid; diisobutylaluminium hydride; trimethyl orthoformate; In dichloromethane; toluene;

DOI:10.1055/s-0033-1338503

upstream raw materials:

2-deoxy-D-ribose

(E)-(5S,6R)-5,6,7-Trihydroxy-2-methyl-hept-2-enoic acid ethyl ester

C₁₇H₂₂O₅

Downstream raw materials:

(2R,4S,5R)-4-((2R,3R)-3-Hydroxymethyl-3-methyl-oxiranylmethyl)-2-phenyl-[1,3]dioxan-5-ol

(2R,4S,5R)-4-((2R,3R)-3-Methyl-3-vinyl-oxiranylmethyl)-2-phenyl-[1,3]dioxan-5-ol

(2R,4aR,6S,7R,8aS)-6-Methyl-2-phenyl-6-vinyl-hexahydro-pyrano[3,2-d][1,3]dioxin-7-ol