Technology Process of C38H55N5O6
There total 12 articles about C38H55N5O6 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
triethylamine;
In
tetrahydrofuran;
for 12h;
Inert atmosphere;
Reflux;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 20 °C / Inert atmosphere
2: diisobutylaluminium hydride / dichloromethane / 4 h / -78 - 20 °C / Inert atmosphere
3: triethylamine / tetrahydrofuran / 12 h / Inert atmosphere; Reflux
With
diisobutylaluminium hydride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; N-ethyl-N,N-diisopropylamine;
In
tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ml400187w
- Guidance literature:
-
Multi-step reaction with 4 steps
1: potassium carbonate / tetrahydrofuran / 20 °C / Inert atmosphere
2: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 20 °C / Inert atmosphere
3: diisobutylaluminium hydride / dichloromethane / 4 h / -78 - 20 °C / Inert atmosphere
4: triethylamine / tetrahydrofuran / 12 h / Inert atmosphere; Reflux
With
diisobutylaluminium hydride; potassium carbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; N-ethyl-N,N-diisopropylamine;
In
tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ml400187w
