3-<3-(2'-Furyl)-2,2-bis(phenylsulfonyl)propyl>-2,5,6-trimethyl-4H-pyran-4-one

Base Information

Chemical Name:3-<3-(2'-Furyl)-2,2-bis(phenylsulfonyl)propyl>-2,5,6-trimethyl-4H-pyran-4-one
CAS No.:151831-99-1
Molecular Formula:C₂₇H₂₆O₇S₂
Molecular Weight:526.631
Hs Code.:

Synonyms:3-<3-(2'-Furyl)-2,2-bis(phenylsulfonyl)propyl>-2,5,6-trimethyl-4H-pyran-4-one

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Chemical Property of 3-<3-(2'-Furyl)-2,2-bis(phenylsulfonyl)propyl>-2,5,6-trimethyl-4H-pyran-4-one

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Technology Process of 3-<3-(2'-Furyl)-2,2-bis(phenylsulfonyl)propyl>-2,5,6-trimethyl-4H-pyran-4-one

There total 5 articles about 3-<3-(2'-Furyl)-2,2-bis(phenylsulfonyl)propyl>-2,5,6-trimethyl-4H-pyran-4-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 151831-96-8
3-(Bromomethyl)-2,5,6-trimethyl-4H-pyran-4-one

: 151831-95-7
2,2-Bis(phenylsulfonyl)-1-(2'-furyl)ethane

: 151831-99-1
3-<3-(2'-Furyl)-2,2-bis(phenylsulfonyl)propyl>-2,5,6-trimethyl-4H-pyran-4-one

Guidance literature:: With sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate; In dichloromethane; for 12h; Ambient temperature;
DOI:10.1021/jo00076a047

Reference yield:

: 98-01-1
furfural

: 151831-99-1
3-<3-(2'-Furyl)-2,2-bis(phenylsulfonyl)propyl>-2,5,6-trimethyl-4H-pyran-4-one

Guidance literature:: Multi-step reaction with 3 steps

1: methanol

2: 99 percent / NaBH₄ / methanol / 1 h / Ambient temperature

3: 92 percent / aq. NaOH / tetrabutylammonium hydrogen sulfate / CH₂Cl₂ / 12 h / Ambient temperature

With sodium hydroxide; sodium tetrahydroborate; tetra(n-butyl)ammonium hydrogensulfate; In methanol; dichloromethane;
DOI:10.1021/jo00076a047

Reference yield:

: 14901-87-2
2,3,5,6-Tetramethyl-4H-pyran-4-one

: 151831-99-1
3-<3-(2'-Furyl)-2,2-bis(phenylsulfonyl)propyl>-2,5,6-trimethyl-4H-pyran-4-one

Guidance literature:: Multi-step reaction with 2 steps

1: 72 percent / N-bromosuccinimide / benzoyl peroxide / CCl₄ / 2 h / Heating

2: 92 percent / aq. NaOH / tetrabutylammonium hydrogen sulfate / CH₂Cl₂ / 12 h / Ambient temperature

With sodium hydroxide; N-Bromosuccinimide; tetra(n-butyl)ammonium hydrogensulfate; dibenzoyl peroxide; In tetrachloromethane; dichloromethane;
DOI:10.1021/jo00076a047