C₅₄H₆₅N₅O₂₀

Base Information

Chemical Name:C₅₄H₆₅N₅O₂₀
CAS No.:1313375-36-8
Molecular Formula:C₅₄H₆₅N₅O₂₀
Molecular Weight:1104.13
Hs Code.:

C<sub>54</sub>H<sub>65</sub>N<sub>5</sub>O<sub>20</sub>

Synonyms:C₅₄H₆₅N₅O₂₀

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Chemical Property of C₅₄H₆₅N₅O₂₀

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Technology Process of C₅₄H₆₅N₅O₂₀

There total 7 articles about C₅₄H₆₅N₅O₂₀ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1313375-90-4
C₂₇H₃₁NO₁₀

: 1313375-91-5
C₂₇H₃₄N₄O₁₀

: 1313375-36-8
C₅₄H₆₅N₅O₂₀

Guidance literature:: With copper(ll) sulfate pentahydrate; sodium L-ascorbate; In tetrahydrofuran; water; at 20 - 50 ℃; for 21h; Inert atmosphere;
DOI:10.1002/chem.201003402

Reference yield:

: 1071472-86-0
methyl (E)-4-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-but-2-enoate

: 1313375-36-8
C₅₄H₆₅N₅O₂₀

Guidance literature:: Multi-step reaction with 5 steps

1.1: tetrabutylammomium bromide; palladium diacetate; sodium hydrogencarbonate / N,N-dimethyl-formamide / 8 h / 85 °C / Inert atmosphere

2.1: sodium methylate / methanol / 24 h / 20 °C

3.1: water; lithium hydroxide / tetrahydrofuran; methanol; water / 3 h / 20 °C / Inert atmosphere

4.1: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 0 - 20 °C

4.2: 20 °C

5.1: copper(ll) sulfate pentahydrate; sodium L-ascorbate / tetrahydrofuran; water / 21 h / 20 - 50 °C / Inert atmosphere

With copper(ll) sulfate pentahydrate; tetrabutylammomium bromide; water; sodium methylate; palladium diacetate; sodium hydrogencarbonate; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; sodium L-ascorbate; N-ethyl-N,N-diisopropylamine; lithium hydroxide; In tetrahydrofuran; methanol; water; N,N-dimethyl-formamide; 1.1: Heck coupling / 2.1: Zemplen reaction;
DOI:10.1002/chem.201003402

Reference yield:

: 53263-18-6,82659-53-8,98920-44-6,98920-46-8,98920-49-1,103773-87-1,98920-48-0
3-(1'-deoxy-2',3',4',6'-tetra-O-acetyl-β-D-galactopyranosyl)prop-1-ene

: 1313375-36-8
C₅₄H₆₅N₅O₂₀

Guidance literature:: Multi-step reaction with 6 steps

1.1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / dichloromethane / 3 h / 45 °C / Inert atmosphere

2.1: tetrabutylammomium bromide; palladium diacetate; sodium hydrogencarbonate / N,N-dimethyl-formamide / 8 h / 85 °C / Inert atmosphere

3.1: sodium methylate / methanol / 24 h / 20 °C

4.1: water; lithium hydroxide / tetrahydrofuran; methanol; water / 3 h / 20 °C / Inert atmosphere

5.1: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 0 - 20 °C

5.2: 20 °C

6.1: copper(ll) sulfate pentahydrate; sodium L-ascorbate / tetrahydrofuran; water / 21 h / 20 - 50 °C / Inert atmosphere

With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; copper(ll) sulfate pentahydrate; tetrabutylammomium bromide; water; sodium methylate; palladium diacetate; sodium hydrogencarbonate; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; sodium L-ascorbate; N-ethyl-N,N-diisopropylamine; lithium hydroxide; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide; 2.1: Heck coupling / 3.1: Zemplen reaction;
DOI:10.1002/chem.201003402