5-[4''-(2-cyanoethyl)-2'',6''-dimethylphenoxy]-N¹-(4'-cyanophenyl)-4-(methoxymethyl)benzene-1,2-diamine

Base Information

• Chemical Name: 5-[4''-(2-cyanoethyl)-2'',6''-dimethylphenoxy]-N¹-(4'-cyanophenyl)-4-(methoxymethyl)benzene-1,2-diamine
• CAS No.: 1539287-51-8
• Molecular Formula: C₂₆H₂₆N₄O₂
• Molecular Weight: 426.518
• Mol file: 1539287-51-8.mol

Synonyms:5-[4''-(2-cyanoethyl)-2'',6''-dimethylphenoxy]-N¹-(4'-cyanophenyl)-4-(methoxymethyl)benzene-1,2-diamine

Chemical Property of 5-[4''-(2-cyanoethyl)-2'',6''-dimethylphenoxy]-N¹-(4'-cyanophenyl)-4-(methoxymethyl)benzene-1,2-diamine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 5-[4''-(2-cyanoethyl)-2'',6''-dimethylphenoxy]-N¹-(4'-cyanophenyl)-4-(methoxymethyl)benzene-1,2-diamine

There total 13 articles about 5-[4''-(2-cyanoethyl)-2'',6''-dimethylphenoxy]-N¹-(4'-cyanophenyl)-4-(methoxymethyl)benzene-1,2-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

C26H22N4O4 (1622438-20-3) → 5-[4''-(2-cyanoethyl)-2'',6''-dimethylphenoxy]-N1-(4'-cyanophenyl)-4-(methoxymethyl)benzene-1,2-diamine (1539287-51-8)

Guidance literature:

With 5%-palladium/activated carbon; hydrogen; In ethanol; for 0.4h; under 2585.81 - 2844.39 Torr;

DOI:10.1016/j.bmcl.2014.07.011

Reference yield: 79.0%

N1-(4'-cyanophenyl)-5-[4''-(2-cyanovinyl)-2'',6''-dimethylphenoxy]-4-methoxymethyl-2-nitroaniline → 5-[4''-(2-cyanoethyl)-2'',6''-dimethylphenoxy]-N1-(4'-cyanophenyl)-4-(methoxymethyl)benzene-1,2-diamine (1539287-51-8)

Guidance literature:

With palladium 10% on activated carbon; hydrogen;

DOI:10.1021/acs.jmedchem.5b01827

Reference yield: 79.0%

→ 5-[4''-(2-cyanoethyl)-2'',6''-dimethylphenoxy]-N1-(4'-cyanophenyl)-4-(methoxymethyl)benzene-1,2-diamine (1539287-51-8)

Guidance literature:

With 5%-palladium/activated carbon; hydrogen; In ethanol; for 2h; under 1551.49 - 2068.65 Torr;

upstream raw materials:

N¹-(4-cyanophenyl)-5-(4'-cyanovinyl-2',6'-dimethylphenoxy)-4-hydroxymethyl-2-nitroaniline

C₂₆H₂₂N₄O₄

4-hydroxy-3,5-dimethylbenzaldehyde

3,5-dimethyl-4-benzyloxy benzaldehyde