((5-bromo-2,3-bis-methoxycarbonyloxy-benzoyl)-{3-[(5-bromo-2,3-bis-methoxycarbonyloxy-benzoyl)-methyl-amino]-propyl}-amino)-acetic acid

Base Information

Chemical Name:((5-bromo-2,3-bis-methoxycarbonyloxy-benzoyl)-{3-[(5-bromo-2,3-bis-methoxycarbonyloxy-benzoyl)-methyl-amino]-propyl}-amino)-acetic acid
CAS No.:439216-86-1
Molecular Formula:C₂₈H₂₈Br₂N₂O₁₆
Molecular Weight:808.342
Hs Code.:

Synonyms:((5-bromo-2,3-bis-methoxycarbonyloxy-benzoyl)-{3-[(5-bromo-2,3-bis-methoxycarbonyloxy-benzoyl)-methyl-amino]-propyl}-amino)-acetic acid

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Chemical Property of ((5-bromo-2,3-bis-methoxycarbonyloxy-benzoyl)-{3-[(5-bromo-2,3-bis-methoxycarbonyloxy-benzoyl)-methyl-amino]-propyl}-amino)-acetic acid

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Technology Process of ((5-bromo-2,3-bis-methoxycarbonyloxy-benzoyl)-{3-[(5-bromo-2,3-bis-methoxycarbonyloxy-benzoyl)-methyl-amino]-propyl}-amino)-acetic acid

There total 1 articles about ((5-bromo-2,3-bis-methoxycarbonyloxy-benzoyl)-{3-[(5-bromo-2,3-bis-methoxycarbonyloxy-benzoyl)-methyl-amino]-propyl}-amino)-acetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 439216-79-2
5-bromo-2,3-di(methoxycarbonyloxy)benzoyl chloride

: 439216-71-4
N-(methylaminopropyl)glycine

: 439216-86-1
((5-bromo-2,3-bis-methoxycarbonyloxy-benzoyl)-{3-[(5-bromo-2,3-bis-methoxycarbonyloxy-benzoyl)-methyl-amino]-propyl}-amino)-acetic acid

Guidance literature:: With sodium hydrogencarbonate; In tetrahydrofuran; at 0 - 5 ℃; for 1h;
DOI:10.1021/jm010546b

Reference yield:

: 79-22-1
methyl chloroformate

: 439216-86-1
((5-bromo-2,3-bis-methoxycarbonyloxy-benzoyl)-{3-[(5-bromo-2,3-bis-methoxycarbonyloxy-benzoyl)-methyl-amino]-propyl}-amino)-acetic acid

: C₃₀H₃₀Br₂N₂O₁₈

Guidance literature:: With 4-methyl-morpholine; In tetrahydrofuran; at -20 - -10 ℃; for 1h;
DOI:10.1021/jm010546b

Reference yield:

: 439216-86-1
((5-bromo-2,3-bis-methoxycarbonyloxy-benzoyl)-{3-[(5-bromo-2,3-bis-methoxycarbonyloxy-benzoyl)-methyl-amino]-propyl}-amino)-acetic acid

: N-[N',N''-bis-(2,3-dimethoxycarbonyloxy-5-bromo-benzoyl)-N-(methylaminopropyl)glycyl]ampicillin

Guidance literature:: Multi-step reaction with 2 steps

1: N-methylmorpholine / tetrahydrofuran / 1 h / -20 - -10 °C

2: triethylamine / tetrahydrofuran; H₂O / 2 h / -20 - 20 °C

With 4-methyl-morpholine; triethylamine; In tetrahydrofuran; water;
DOI:10.1021/jm010546b