3-(2-chlorophenyl)-6-(4-methoxyphenyl)-5-methylthieno[2,3-d]pyrimidine-2,4(1H,3H)-dione

Base Information

Chemical Name:3-(2-chlorophenyl)-6-(4-methoxyphenyl)-5-methylthieno[2,3-d]pyrimidine-2,4(1H,3H)-dione
CAS No.:174072-98-1
Molecular Formula:C₂₀H₁₅ClN₂O₃S
Molecular Weight:398.87
Hs Code.:

Synonyms:3-(2-chlorophenyl)-6-(4-methoxyphenyl)-5-methylthieno[2,3-d]pyrimidine-2,4(1H,3H)-dione

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Chemical Property of 3-(2-chlorophenyl)-6-(4-methoxyphenyl)-5-methylthieno[2,3-d]pyrimidine-2,4(1H,3H)-dione

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Technology Process of 3-(2-chlorophenyl)-6-(4-methoxyphenyl)-5-methylthieno[2,3-d]pyrimidine-2,4(1H,3H)-dione

There total 3 articles about 3-(2-chlorophenyl)-6-(4-methoxyphenyl)-5-methylthieno[2,3-d]pyrimidine-2,4(1H,3H)-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 122-84-9
4-methoxybenzyl methyl ketone

: 174072-98-1
3-(2-chlorophenyl)-6-(4-methoxyphenyl)-5-methylthieno[2,3-d]pyrimidine-2,4(1H,3H)-dione

Guidance literature:: Multi-step reaction with 3 steps

1.1: NH₄OAc; AcOH / toluene / 20 h / Heating

1.2: 40 percent / sulfur / ethanol / 2 h / 65 °C

2.1: pyridine / 45 °C

3.1: NaOMe / methanol / 20 °C

With pyridine; ammonium acetate; sodium methylate; acetic acid; In methanol; toluene;
DOI:10.1021/jm020180i

Reference yield:

: 3320-83-0
o-chlorophenyl isocyanate

: 174072-98-1
3-(2-chlorophenyl)-6-(4-methoxyphenyl)-5-methylthieno[2,3-d]pyrimidine-2,4(1H,3H)-dione

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / 45 °C

2: NaOMe / methanol / 20 °C

With pyridine; sodium methylate; In methanol;
DOI:10.1021/jm020180i

Reference yield:

: 165809-38-1
2-amino-4-methyl-5-(4-methoxyphenyl)thiophene-3-carboxylic acid ethyl ester

: 174072-98-1
3-(2-chlorophenyl)-6-(4-methoxyphenyl)-5-methylthieno[2,3-d]pyrimidine-2,4(1H,3H)-dione

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / 45 °C

2: NaOMe / methanol / 20 °C

With pyridine; sodium methylate; In methanol;
DOI:10.1021/jm020180i