1-[1'-(benzyloxycarbonylamino)ethyl]-6,7-dimethoxy-3,4-dihydroisoquinoline

Base Information

Chemical Name:1-[1'-(benzyloxycarbonylamino)ethyl]-6,7-dimethoxy-3,4-dihydroisoquinoline
CAS No.:66659-39-0
Molecular Formula:C₂₁H₂₄N₂O₄
Molecular Weight:368.433
Hs Code.:

Synonyms:1-[1'-(benzyloxycarbonylamino)ethyl]-6,7-dimethoxy-3,4-dihydroisoquinoline

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Chemical Property of 1-[1'-(benzyloxycarbonylamino)ethyl]-6,7-dimethoxy-3,4-dihydroisoquinoline

Chemical Property:

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Technology Process of 1-[1'-(benzyloxycarbonylamino)ethyl]-6,7-dimethoxy-3,4-dihydroisoquinoline

There total 4 articles about 1-[1'-(benzyloxycarbonylamino)ethyl]-6,7-dimethoxy-3,4-dihydroisoquinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 72020-37-2
2-benzyloxycarbonylamino-N-[2-(3,4-dimethoxyphenyl)ethyl]propanamide

: 66659-39-0
1-[1'-(benzyloxycarbonylamino)ethyl]-6,7-dimethoxy-3,4-dihydroisoquinoline

Guidance literature:: With trichlorophosphate; In chloroform; for 3h; Reflux;
DOI:10.3998/ark.5550190.0013.521

Reference yield:

: 4132-86-9,26607-51-2,1142-20-7
N-benzyloxycarbonylalanine

: 66659-39-0
1-[1'-(benzyloxycarbonylamino)ethyl]-6,7-dimethoxy-3,4-dihydroisoquinoline

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / toluene / 0.08 h / -10 °C

2: toluene; dichloromethane / 0.08 h / 0 °C / Reflux

3: trichlorophosphate / chloroform / 3 h / Reflux

With triethylamine; trichlorophosphate; In dichloromethane; chloroform; toluene;
DOI:10.3998/ark.5550190.0013.521

Reference yield:

: 112277-33-5
C₁₄H₁₇NO₆

: 66659-39-0
1-[1'-(benzyloxycarbonylamino)ethyl]-6,7-dimethoxy-3,4-dihydroisoquinoline

Guidance literature:: Multi-step reaction with 2 steps

1: toluene; dichloromethane / 0.08 h / 0 °C / Reflux

2: trichlorophosphate / chloroform / 3 h / Reflux

With trichlorophosphate; In dichloromethane; chloroform; toluene;
DOI:10.3998/ark.5550190.0013.521