3-(4-Methylphenyl)-2-propen-1-amine

Base Information

Chemical Name:3-(4-Methylphenyl)-2-propen-1-amine
CAS No.:158223-55-3
Molecular Formula:C₁₀H₁₃N
Molecular Weight:147.22
Hs Code.:
DSSTox Substance ID:DTXSID801276911
Nikkaji Number:J602.499H

Synonyms:158223-55-3;3-(4-Methylphenyl)-2-propen-1-amine;(E)-3-(4-methylphenyl)prop-2-en-1-amine;[(2E)-3-(4-methylphenyl)prop-2-en-1-yl]amine;2-Propen-1-amine, 3-(4-methylphenyl)-, (2E)-;3-(4-methylphenyl)prop-2-en-1-amine;SCHEMBL11762473;DTXSID801276911;MFCD19623073;(E)-3-(P-tolyl)prop-2-en-1-amine;BS-12595;CS-0281118;(2E)-3-(4-Methylphenyl)-2-propen-1-amine;EN300-1246784

Suppliers and Price of 3-(4-Methylphenyl)-2-propen-1-amine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of 3-(4-Methylphenyl)-2-propen-1-amine

Chemical Property:

XLogP3:1.8
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:2
Exact Mass:147.104799419
Heavy Atom Count:11
Complexity:121

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC1=CC=C(C=C1)C=CCN
Isomeric SMILES:CC1=CC=C(C=C1)/C=C/CN

Technology Process of 3-(4-Methylphenyl)-2-propen-1-amine

There total 9 articles about 3-(4-Methylphenyl)-2-propen-1-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 22553-96-4
(E)-2-(3-(4-methylphenyl)prop-2-enyl)isoindoline-1,3-dione

: 158223-55-3
(E)-3-(4-methylphenyl)prop-2-en-1-amine

Guidance literature:: With ethanol; hydrazine hydrate; for 3h; Reflux;
DOI:10.1016/j.tet.2009.04.007

Reference yield: 49.0%

: 56578-35-9
4-methyl-cinnamaldehyde

: 158223-55-3
(E)-3-(4-methylphenyl)prop-2-en-1-amine

Guidance literature:: With (S)-1-phenyl-ethylamine; pyridoxal 5'-phosphate; pQR₁₁₀₈; In aq. phosphate buffer; dimethyl sulfoxide; at 30 ℃; for 18h; pH=8; Enzymatic reaction;
DOI:10.1039/c6gc02769e

Reference yield:

: 2749-96-4
4-methylphenylallene

: 158223-55-3
(E)-3-(4-methylphenyl)prop-2-en-1-amine

Guidance literature:: Multi-step reaction with 2 steps

1: 99 percent / Pd₂(DBA)3*CHCl₃, dppf / tetrahydrofuran; acetic acid / 8 h / 80 °C

2: 1.) β,β,β-trichloroethyl chloroformate, 2.) zinc / 1.) CH3CN, 2.) acetic acid

With zinc; 2,2,2-Trichloroethyl chloroformate; tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; 1,1'-bis-(diphenylphosphino)ferrocene; In tetrahydrofuran; acetic acid;
DOI:10.1016/S0040-4039(97)01370-1