1,8,9,20-Tetrahydro-3,6-dimethyl-1,8-diphenyldibenzodipyrazolo<5,4-f:4',5'-j><1,2,5,8,9,12>hexaazacyclotetradecene

Base Information

Chemical Name:1,8,9,20-Tetrahydro-3,6-dimethyl-1,8-diphenyldibenzodipyrazolo<5,4-f:4',5'-j><1,2,5,8,9,12>hexaazacyclotetradecene
CAS No.:90167-31-0
Molecular Formula:C₃₂H₂₆N₁₀
Molecular Weight:550.625
Hs Code.:

1,8,9,20-Tetrahydro-3,6-dimethyl-1,8-diphenyldibenzo<c,m>dipyrazolo<5,4-f:4',5'-j><1,2,5,8,9,12>hexaazacyclotetradecene

Synonyms:1,8,9,20-Tetrahydro-3,6-dimethyl-1,8-diphenyldibenzodipyrazolo<5,4-f:4',5'-j><1,2,5,8,9,12>hexaazacyclotetradecene

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Chemical Property of 1,8,9,20-Tetrahydro-3,6-dimethyl-1,8-diphenyldibenzodipyrazolo<5,4-f:4',5'-j><1,2,5,8,9,12>hexaazacyclotetradecene

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Technology Process of 1,8,9,20-Tetrahydro-3,6-dimethyl-1,8-diphenyldibenzodipyrazolo<5,4-f:4',5'-j><1,2,5,8,9,12>hexaazacyclotetradecene

There total 1 articles about 1,8,9,20-Tetrahydro-3,6-dimethyl-1,8-diphenyldibenzodipyrazolo<5,4-f:4',5'-j><1,2,5,8,9,12>hexaazacyclotetradecene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 60997-47-9
4,4'-azobis<5-chloro-3-methyl-1-phenylpyrazole>

: 90167-31-0
1,8,9,20-Tetrahydro-3,6-dimethyl-1,8-diphenyldibenzodipyrazolo<5,4-f:4',5'-j><1,2,5,8,9,12>hexaazacyclotetradecene

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / xylene / 3 h / 130 - 140 °C

2: 30 percent / MgO / dimethylformamide / 6 h / 130 - 140 °C

With magnesium oxide; In N,N-dimethyl-formamide; xylene;
DOI:10.1007/BF00506292