N₂-(tert-butoxycarbonyl)glycyl-N₂-(2,4-dimethoxybenzyl)-N₁-[(1S)-1-methyl-2-(4-[(1RS)-3,3,3-trifluoro-2-hydroxy-2-(methoxycarbonyl)propyl]-1H-1,2,3-triazol-1-yl)ethyl]glycinamide

Base Information

• Chemical Name: N₂-(tert-butoxycarbonyl)glycyl-N₂-(2,4-dimethoxybenzyl)-N₁-[(1S)-1-methyl-2-(4-[(1RS)-3,3,3-trifluoro-2-hydroxy-2-(methoxycarbonyl)propyl]-1H-1,2,3-triazol-1-yl)ethyl]glycinamide
• CAS No.: 1360464-80-7
• Molecular Formula: C₂₈H₃₉F₃N₆O₉
• Molecular Weight: 660.648

Synonyms:N₂-(tert-butoxycarbonyl)glycyl-N₂-(2,4-dimethoxybenzyl)-N₁-[(1S)-1-methyl-2-(4-[(1RS)-3,3,3-trifluoro-2-hydroxy-2-(methoxycarbonyl)propyl]-1H-1,2,3-triazol-1-yl)ethyl]glycinamide

Chemical Property of N₂-(tert-butoxycarbonyl)glycyl-N₂-(2,4-dimethoxybenzyl)-N₁-[(1S)-1-methyl-2-(4-[(1RS)-3,3,3-trifluoro-2-hydroxy-2-(methoxycarbonyl)propyl]-1H-1,2,3-triazol-1-yl)ethyl]glycinamide

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Technology Process of N₂-(tert-butoxycarbonyl)glycyl-N₂-(2,4-dimethoxybenzyl)-N₁-[(1S)-1-methyl-2-(4-[(1RS)-3,3,3-trifluoro-2-hydroxy-2-(methoxycarbonyl)propyl]-1H-1,2,3-triazol-1-yl)ethyl]glycinamide

There total 1 articles about N₂-(tert-butoxycarbonyl)glycyl-N₂-(2,4-dimethoxybenzyl)-N₁-[(1S)-1-methyl-2-(4-[(1RS)-3,3,3-trifluoro-2-hydroxy-2-(methoxycarbonyl)propyl]-1H-1,2,3-triazol-1-yl)ethyl]glycinamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

N-(tert-butoxycarbonyl)glycyl-N1-[(1S)-2-azido-1-methylethyl]-N2-(2,4-dimethoxybenzyl)glycinamide (1316672-54-4) + methyl 2-hydroxy-2-trifluoromethylpent-4-ynoate (537034-30-3) → N2-(tert-butoxycarbonyl)glycyl-N2-(2,4-dimethoxybenzyl)-N1-[(1S)-1-methyl-2-(4-[(1RS)-3,3,3-trifluoro-2-hydroxy-2-(methoxycarbonyl)propyl]-1H-1,2,3-triazol-1-yl)ethyl]glycinamide (1360464-80-7)

Guidance literature:

With copper(ll) sulfate pentahydrate; sodium L-ascorbate; In dichloromethane; water; at 40 ℃; for 3h; regioselective reaction;

DOI:10.1055/s-0031-1289609

upstream raw materials:

N-(tert-butoxycarbonyl)glycyl-N₁-[(1S)-2-azido-1-methylethyl]-N₂-(2,4-dimethoxybenzyl)glycinamide

methyl 2-hydroxy-2-trifluoromethylpent-4-ynoate

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