1-(2,3,5-Tri-O-benzyl-β-D-ribofuranosyl)-1H-1,2,4-triazol-3-carbonsaeure-ethylester

Base Information

Chemical Name:1-(2,3,5-Tri-O-benzyl-β-D-ribofuranosyl)-1H-1,2,4-triazol-3-carbonsaeure-ethylester
CAS No.:79437-72-2
Molecular Formula:C₃₁H₃₃N₃O₆
Molecular Weight:543.62
Hs Code.:

Synonyms:1-(2,3,5-Tri-O-benzyl-β-D-ribofuranosyl)-1H-1,2,4-triazol-3-carbonsaeure-ethylester

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Chemical Property of 1-(2,3,5-Tri-O-benzyl-β-D-ribofuranosyl)-1H-1,2,4-triazol-3-carbonsaeure-ethylester

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Technology Process of 1-(2,3,5-Tri-O-benzyl-β-D-ribofuranosyl)-1H-1,2,4-triazol-3-carbonsaeure-ethylester

There total 1 articles about 1-(2,3,5-Tri-O-benzyl-β-D-ribofuranosyl)-1H-1,2,4-triazol-3-carbonsaeure-ethylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 79437-73-3
Amino(2,3,5-Tri-O-benzyl-D-ribofuranosylhydrazono)essigsaeure-ethylester

: 122-51-0
orthoformic acid triethyl ester

: 79437-72-2
1-(2,3,5-Tri-O-benzyl-β-D-ribofuranosyl)-1H-1,2,4-triazol-3-carbonsaeure-ethylester

Guidance literature:: In toluene; at 100 ℃; for 4h; Yield given;
DOI:10.1002/cber.19811140814

Reference yield: 100.0%

: 79437-72-2
1-(2,3,5-Tri-O-benzyl-β-D-ribofuranosyl)-1H-1,2,4-triazol-3-carbonsaeure-ethylester

: 72933-99-4
1-(2,3,5-Tri-O-benzyl-β-D-ribofuranosyl)-1H-1,2,4-triazol-3-carboxamid

Guidance literature:: With ammonia; In methanol; for 12h; Ambient temperature;
DOI:10.1002/cber.19811140814

Reference yield:

: 79437-72-2
1-(2,3,5-Tri-O-benzyl-β-D-ribofuranosyl)-1H-1,2,4-triazol-3-carbonsaeure-ethylester

: 36791-04-5,66510-90-5
ribavirin

Guidance literature:: Multi-step reaction with 2 steps

1: H₂, 9.5 N ethanolic HCl / Pd / ethanol / 10 h

2: 76 percent / NH₃ / methanol / Ambient temperature

With hydrogenchloride; ammonia; hydrogen; palladium; In methanol; ethanol;
DOI:10.1002/cber.19811140814