Technology Process of C32H44N4O9
There total 5 articles about C32H44N4O9 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; triethylamine;
In
dichloromethane;
for 0.333333h;
DOI:10.1021/ol201282d
- Guidance literature:
-
Multi-step reaction with 2 steps
1: iron; acetic acid / dichloromethane / 4 h / 20 °C
2: bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; triethylamine / dichloromethane / 0.33 h
With
bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; iron; acetic acid; triethylamine;
In
dichloromethane;
DOI:10.1021/ol201282d
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / dichloromethane / 0.5 h / 20 °C / Inert atmosphere
1.2: 20 °C / Inert atmosphere
2.1: water; sodium hydroxide / 12 h / 60 °C
3.1: bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; triethylamine / dichloromethane / 0.33 h
With
water; bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; sodium hydroxide;
In
dichloromethane;
DOI:10.1021/ol201282d