2-(tosyloxy)ethyl 8-[(2E)-3-iodoprop-2-en-1-yl]-3-(4-methyl-phenyl)-8-azabicyclo[3.2.1]octane-2-carboxylate

Base Information

Chemical Name:2-(tosyloxy)ethyl 8-[(2E)-3-iodoprop-2-en-1-yl]-3-(4-methyl-phenyl)-8-azabicyclo[3.2.1]octane-2-carboxylate
CAS No.:1391711-43-5
Molecular Formula:C₂₇H₃₂INO₅S
Molecular Weight:609.525
Hs Code.:

Synonyms:2-(tosyloxy)ethyl 8-[(2E)-3-iodoprop-2-en-1-yl]-3-(4-methyl-phenyl)-8-azabicyclo[3.2.1]octane-2-carboxylate

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Chemical Property of 2-(tosyloxy)ethyl 8-[(2E)-3-iodoprop-2-en-1-yl]-3-(4-methyl-phenyl)-8-azabicyclo[3.2.1]octane-2-carboxylate

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Technology Process of 2-(tosyloxy)ethyl 8-[(2E)-3-iodoprop-2-en-1-yl]-3-(4-methyl-phenyl)-8-azabicyclo[3.2.1]octane-2-carboxylate

There total 1 articles about 2-(tosyloxy)ethyl 8-[(2E)-3-iodoprop-2-en-1-yl]-3-(4-methyl-phenyl)-8-azabicyclo[3.2.1]octane-2-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: 311351-26-5
C₁₈H₂₂INO₂

: 6315-52-2
1,2-bis-tosyloxyethane

: 1391711-43-5
2-(tosyloxy)ethyl 8-[(2E)-3-iodoprop-2-en-1-yl]-3-(4-methyl-phenyl)-8-azabicyclo[3.2.1]octane-2-carboxylate

Guidance literature:: C₁₈H₂₂INO₂; With tetra(n-butyl)ammonium hydroxide; In water; toluene; at 20 ℃; for 0.166667h;

1,2-bis-tosyloxyethane; In acetonitrile; at 20 ℃; for 2h;
DOI:10.1002/jlcr.2927

Reference yield:

: 1391711-43-5
2-(tosyloxy)ethyl 8-[(2E)-3-iodoprop-2-en-1-yl]-3-(4-methyl-phenyl)-8-azabicyclo[3.2.1]octane-2-carboxylate

: 1187432-35-4
[(18)F]-(E)-N-(3-iodoprop-2-enyl)-2β-carbofluoroethoxy-3β-(4'-methylphenyl)nortropane

Guidance literature:: With potassium carbonate; [2.2.2]cryptande; [18F]fluoride ion, cyclotron produced, NCA; In dimethyl sulfoxide; at 140 ℃; for 0.0833333h;
DOI:10.1002/jlcr.2927