(6R,αR)-2-Methyl-6-heptan-2-ol

Base Information

Chemical Name:(6R,αR)-2-Methyl-6-heptan-2-ol
CAS No.:177329-66-7
Molecular Formula:C₁₇H₂₉NO₂
Molecular Weight:279.423
Hs Code.:

(6R,αR)-2-Methyl-6-<N-methyl-N-(α-methylbenzyl)aminooxy>heptan-2-ol

Synonyms:(6R,αR)-2-Methyl-6-heptan-2-ol

Suppliers and Price of (6R,αR)-2-Methyl-6-heptan-2-ol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (6R,αR)-2-Methyl-6-heptan-2-ol

Chemical Property:

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Technology Process of (6R,αR)-2-Methyl-6-heptan-2-ol

There total 7 articles about (6R,αR)-2-Methyl-6-heptan-2-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 177329-65-6
(6R,αR)-(E)-2-Methyl-6-hept-4-en-2-ol

: 177329-66-7
(6R,αR)-2-Methyl-6-heptan-2-ol

Guidance literature:: With hydrogen; Rh/Al₂O₃; In ethanol;
DOI:10.1016/0957-4166(96)00103-6

Reference yield:

: 177329-63-4
(3S,αR)-(E)-Methyl 3-hex-4-enoate

: 177329-66-7
(6R,αR)-2-Methyl-6-heptan-2-ol

Guidance literature:: Multi-step reaction with 3 steps

1: 93 percent / tetrahydrofuran / 3 h / 20 °C

2: 1.) MCPBA / 1.) CHCl₃, 0 deg C, 30 min, 2.) r.t., 24 h

3: 86 percent / H₂ / 5percent Rh/Al₂O₃ / ethanol / 20 h / 20 °C / 4560 Torr

With hydrogen; 3-chloro-benzenecarboperoxoic acid; Rh/Al₂O₃; In tetrahydrofuran; ethanol;
DOI:10.1039/p19960002467

Reference yield:

: 177329-64-5
(4S,αR)-(E)-2-Methyl-4-hept-5-en-2-ol

: 177329-66-7
(6R,αR)-2-Methyl-6-heptan-2-ol

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) MCPBA / 1.) CHCl₃, 0 deg C, 30 min, 2.) r.t., 24 h

2: 86 percent / H₂ / 5percent Rh/Al₂O₃ / ethanol / 20 h / 20 °C / 4560 Torr

With hydrogen; 3-chloro-benzenecarboperoxoic acid; Rh/Al₂O₃; In ethanol;
DOI:10.1039/p19960002467