3,3-dimethyl-N-(2,3,5,6-tetrafluoro-4-(trifluoromethyl)phenyl)pentanamide

Base Information

Chemical Name:3,3-dimethyl-N-(2,3,5,6-tetrafluoro-4-(trifluoromethyl)phenyl)pentanamide
CAS No.:1588498-39-8
Molecular Formula:C₁₄H₁₄F₇NO
Molecular Weight:345.26
Hs Code.:

Synonyms:3,3-dimethyl-N-(2,3,5,6-tetrafluoro-4-(trifluoromethyl)phenyl)pentanamide

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Chemical Property of 3,3-dimethyl-N-(2,3,5,6-tetrafluoro-4-(trifluoromethyl)phenyl)pentanamide

Chemical Property:

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Technology Process of 3,3-dimethyl-N-(2,3,5,6-tetrafluoro-4-(trifluoromethyl)phenyl)pentanamide

There total 2 articles about 3,3-dimethyl-N-(2,3,5,6-tetrafluoro-4-(trifluoromethyl)phenyl)pentanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3177-74-0
3,3-dimethylpentanoic acid

: 1588498-39-8
3,3-dimethyl-N-(2,3,5,6-tetrafluoro-4-(trifluoromethyl)phenyl)pentanamide

Guidance literature:: Multi-step reaction with 2 steps

1: oxalyl dichloride / dichloromethane / 20 °C

2: toluene / 12 h / Reflux

With oxalyl dichloride; In dichloromethane; toluene;
DOI:10.1021/ja501689j

Reference yield:

: 651-83-2
4-trifluoromethyl-2,3,5,6-tetrafluoroaniline

: 79097-84-0
3,3-dimethylpentanoyl chloride

: 1588498-39-8
3,3-dimethyl-N-(2,3,5,6-tetrafluoro-4-(trifluoromethyl)phenyl)pentanamide

Guidance literature:: In toluene; for 12h; Reflux;
DOI:10.1021/ja501689j

Reference yield: 68.0%

: 1588498-39-8
3,3-dimethyl-N-(2,3,5,6-tetrafluoro-4-(trifluoromethyl)phenyl)pentanamide

: 140-88-5,9003-32-1
ethyl acrylate

: ethyl 2-(4-ethyl-4-methyl-6-oxo-1-(2,3,5,6-tetrafluoro-4-(trifluoromethyl)phenyl)piperidin-2-yl)acetate

Guidance literature:: With dipotassium hydrogenphosphate; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; perfluorotoluene; 7-( tert-butyl)-2,5-dimethyl-3,4-dihydro-2H-pyrano[2,3-b]quinoline; oxygen; silver(I) acetate; palladium diacetate; sodium hydrogencarbonate; at 120 ℃; for 20h; under 760.051 Torr; Schlenk technique; Cooling with acetone-dry ice; High pressure; Sealed tube;
DOI:10.1021/ja501689j