L(Me)GeS

Base Information

Chemical Name:L(Me)GeS
CAS No.:452899-47-7
Molecular Formula:C₃₀H₄₄GeN₂S
Molecular Weight:537.349
Hs Code.:

Synonyms:L(Me)GeS

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of L(Me)GeS

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Technology Process of L(Me)GeS

There total 6 articles about L(Me)GeS which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 452899-44-4
(((CH₃)2CH)2C₆H₃NC(CH₃)CHC(CH₃)NC₆H₃(CH(CH₃)2)2)Ge(S)Cl

: 917-54-4
methyllithium

: 452899-47-7
L(Me)GeS

Guidance literature:: In diethyl ether; toluene; soln. of MeLi in ether was added to soln. of Ge-compound in toluene at -42°C, warmed to room temp., stirred for 2 h under N2; filtered, hexane was added, allowed to stand at room temp. for 2 d; elem. anal.;
DOI:10.1039/b211617k

Reference yield: 65.0%

: 477736-39-3
(HC(CMeNC-2,6-i-Pr₂C₆H₃)2)-methylgermanium(II)

: 7704-34-9
sulfur

: 452899-47-7
L(Me)GeS

Guidance literature:: In toluene; (N2); using Schlenk techniques; addn. of soln. of (HC(CMeNC6H3(i-Pr)2)2)GeMe in toluene to stirred suspn. of elemental sulfur; reflux for 4 h; removal of volatiles; washing with n-hexane; extn. with toluene; addn. of n-hexane, crystn. at room temp. for 3 days; elem. anal.;
DOI:10.1021/om0203328