benzyl 2-acetamido-4-azido-3-O-(D-1-carboxyethyl)-2,4-dideoxy-α-D-glucopyranoside

Base Information

Chemical Name:benzyl 2-acetamido-4-azido-3-O-(D-1-carboxyethyl)-2,4-dideoxy-α-D-glucopyranoside
CAS No.:82827-88-1
Molecular Formula:C₁₈H₂₄N₄O₇
Molecular Weight:408.411
Hs Code.:

Synonyms:benzyl 2-acetamido-4-azido-3-O-(D-1-carboxyethyl)-2,4-dideoxy-α-D-glucopyranoside

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Chemical Property of benzyl 2-acetamido-4-azido-3-O-(D-1-carboxyethyl)-2,4-dideoxy-α-D-glucopyranoside

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Technology Process of benzyl 2-acetamido-4-azido-3-O-(D-1-carboxyethyl)-2,4-dideoxy-α-D-glucopyranoside

There total 3 articles about benzyl 2-acetamido-4-azido-3-O-(D-1-carboxyethyl)-2,4-dideoxy-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (R)-2-((2S,3R,4R,5S,6S)-3-Acetylamino-5-azido-2-benzyloxy-6-trityloxymethyl-tetrahydro-pyran-4-yloxy)-propionic acid

: 82827-88-1
benzyl 2-acetamido-4-azido-3-O-(D-1-carboxyethyl)-2,4-dideoxy-α-D-glucopyranoside

Guidance literature:: With acetic acid; In water; at 50 ℃; for 0.5h; Yield given; Heating;
DOI:10.1016/S0008-6215(00)80689-8

Reference yield:

: 38416-47-6
benzyl 2-acetamido-4-azido-2,4-dideoxy-6-O-trityl-α-D-glucopyranoside

: 82827-88-1
benzyl 2-acetamido-4-azido-3-O-(D-1-carboxyethyl)-2,4-dideoxy-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) 50 percent sodium hydride in oil; 2.) 2 M hydrochloric acid, pH=3 / dioxane / 1 h / 60 °C

2: 70 percent acetic acid / H₂O / 0.5 h / 50 °C / Heating

With hydrogenchloride; sodium hydride; acetic acid; In 1,4-dioxane; water;
DOI:10.1016/S0008-6215(00)80689-8

Reference yield:

: 38416-50-1
benzyl 2-acetamido-4-azido-2,4-dideoxy-α-D-glucopyranoside

: 82827-88-1
benzyl 2-acetamido-4-azido-3-O-(D-1-carboxyethyl)-2,4-dideoxy-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 84 percent / pyridine / 5 h / 90 - 95 °C / Heating

2: 1.) 50 percent sodium hydride in oil; 2.) 2 M hydrochloric acid, pH=3 / dioxane / 1 h / 60 °C

3: 70 percent acetic acid / H₂O / 0.5 h / 50 °C / Heating

With pyridine; hydrogenchloride; sodium hydride; acetic acid; In 1,4-dioxane; water;
DOI:10.1016/S0008-6215(00)80689-8