methyl 3-[2-(1-tert-butyldimethylsilyloxymethyl)-6-(2,6-dimethoxyphenoxymethyl)phenyl]prop-2-ynoate

Base Information

Chemical Name:methyl 3-[2-(1-tert-butyldimethylsilyloxymethyl)-6-(2,6-dimethoxyphenoxymethyl)phenyl]prop-2-ynoate
CAS No.:1043870-89-8
Molecular Formula:C₂₆H₃₄O₆Si
Molecular Weight:470.638
Hs Code.:

Synonyms:methyl 3-[2-(1-tert-butyldimethylsilyloxymethyl)-6-(2,6-dimethoxyphenoxymethyl)phenyl]prop-2-ynoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 3-[2-(1-tert-butyldimethylsilyloxymethyl)-6-(2,6-dimethoxyphenoxymethyl)phenyl]prop-2-ynoate

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Technology Process of methyl 3-[2-(1-tert-butyldimethylsilyloxymethyl)-6-(2,6-dimethoxyphenoxymethyl)phenyl]prop-2-ynoate

There total 1 articles about methyl 3-[2-(1-tert-butyldimethylsilyloxymethyl)-6-(2,6-dimethoxyphenoxymethyl)phenyl]prop-2-ynoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 1043870-84-3
[2-(tert-butyldimethylsilyloxymethyl)-6-(2,6-dimethoxyphenoxymethyl)phenyl]ethyne

: 79-22-1
methyl chloroformate

: 1043870-89-8
methyl 3-[2-(1-tert-butyldimethylsilyloxymethyl)-6-(2,6-dimethoxyphenoxymethyl)phenyl]prop-2-ynoate

Guidance literature:: [2-(tert-butyldimethylsilyloxymethyl)-6-(2,6-dimethoxyphenoxymethyl)phenyl]ethyne; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 0.5h; Inert atmosphere;

methyl chloroformate; In tetrahydrofuran; hexane; at -78 ℃; for 0.5h; Inert atmosphere;
DOI:10.1039/b801208c

Reference yield: 100.0%

: 1043870-89-8
methyl 3-[2-(1-tert-butyldimethylsilyloxymethyl)-6-(2,6-dimethoxyphenoxymethyl)phenyl]prop-2-ynoate

: 917-54-4
methyllithium

: 1043870-90-1
methyl (Z)-3-[2-(1-tert-butyldimethylsilyloxymethyl)-6-(2,6-dimethoxyphenoxymethyl)phenyl]but-2-enoate

Guidance literature:: methyllithium; With copper(l) iodide; In tetrahydrofuran; diethyl ether; at 0 ℃; for 0.5h; Inert atmosphere;

methyl 3-[2-(1-tert-butyldimethylsilyloxymethyl)-6-(2,6-dimethoxyphenoxymethyl)phenyl]prop-2-ynoate; In tetrahydrofuran; diethyl ether; at -78 - -50 ℃; stereoselective reaction; Inert atmosphere;
DOI:10.1039/b801208c