Technology Process of C58H50N2O8S2
There total 4 articles about C58H50N2O8S2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
triethylamine;
In
N,N-dimethyl-formamide;
at 20 ℃;
for 8h;
Inert atmosphere;
DOI:10.1021/jo101981p
- Guidance literature:
-
Multi-step reaction with 3 steps
1: water; sodium hydroxide / tetrahydrofuran / 8 h / 20 °C
2: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 8.25 h / 20 °C / Cooling with ice
3: triethylamine / N,N-dimethyl-formamide / 8 h / 20 °C / Inert atmosphere
With
water; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; sodium hydroxide;
In
tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1021/jo101981p
- Guidance literature:
-
Multi-step reaction with 4 steps
1: potassium carbonate / acetone / 8 h / Reflux
2: water; sodium hydroxide / tetrahydrofuran / 8 h / 20 °C
3: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 8.25 h / 20 °C / Cooling with ice
4: triethylamine / N,N-dimethyl-formamide / 8 h / 20 °C / Inert atmosphere
With
water; potassium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; sodium hydroxide;
In
tetrahydrofuran; N,N-dimethyl-formamide; acetone;
DOI:10.1021/jo101981p
