C₄₈H₇₄O₁₂SSi₂

Base Information

Chemical Name:C₄₈H₇₄O₁₂SSi₂
CAS No.:153145-43-8
Molecular Formula:C₄₈H₇₄O₁₂SSi₂
Molecular Weight:931.345
Hs Code.:

C<sub>48</sub>H<sub>74</sub>O<sub>12</sub>SSi<sub>2</sub>

Synonyms:C₄₈H₇₄O₁₂SSi₂

Suppliers and Price of C₄₈H₇₄O₁₂SSi₂

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₄₈H₇₄O₁₂SSi₂

Chemical Property:

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Technology Process of C₄₈H₇₄O₁₂SSi₂

There total 15 articles about C₄₈H₇₄O₁₂SSi₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 153145-46-1
C₅₁H₈₂O₁₂SSi₃

: 153145-43-8
C₄₈H₇₄O₁₂SSi₂

Guidance literature:: With acetic acid; at 0 ℃; for 14h; Yield given;

Reference yield:

: 153145-26-7
C₃₂H₅₆O₇Si₂

: 153145-43-8
C₄₈H₇₄O₁₂SSi₂

Guidance literature:: Multi-step reaction with 8 steps

1: 92 percent / EtN(i-Pr)2, (Bu)4NI / CH₂Cl₂ / 32 h / Heating

2: 1.) LDA, 2.) mCPBA / 1.) THF, -78 deg C, 2.) hexane, 25 deg C, 5 h

3: 95 percent / CH₂Cl₂ / 15 h / -45 °C

4: 63 percent / Burgess' reagent

5: 80 percent / OsO₄, pyridine / diethyl ether / 12 h / 0 °C

6: Et₃N / -78 °C

7: LDA / 3 h / -35 °C

8: HOAc / 14 h / 0 °C

With pyridine; osmium(VIII) oxide; Burgess Reagent; tetra-(n-butyl)ammonium iodide; acetic acid; triethylamine; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; lithium diisopropyl amide; In diethyl ether; dichloromethane;

Reference yield:

: 153145-20-1
C₃₄H₅₈O₇Si₂

: 153145-43-8
C₄₈H₇₄O₁₂SSi₂

Guidance literature:: Multi-step reaction with 15 steps

1: O₃

2: KMnO₄, KH₂PO₄

4: 93 percent / LDA / tetrahydrofuran / 0.5 h / -78 °C

5: 100 percent / p-TsOH

6: 92 percent / PhSK / dimethylformamide / 3 h / 86 °C

7: acid

8: 92 percent / EtN(i-Pr)2, (Bu)4NI / CH₂Cl₂ / 32 h / Heating

9: 1.) LDA, 2.) mCPBA / 1.) THF, -78 deg C, 2.) hexane, 25 deg C, 5 h

10: 95 percent / CH₂Cl₂ / 15 h / -45 °C

11: 63 percent / Burgess' reagent

12: 80 percent / OsO₄, pyridine / diethyl ether / 12 h / 0 °C

13: Et₃N / -78 °C

14: LDA / 3 h / -35 °C

15: HOAc / 14 h / 0 °C

With pyridine; potassium permanganate; potassium dihydrogenphosphate; osmium(VIII) oxide; Burgess Reagent; tetra-(n-butyl)ammonium iodide; (2E)-3-(4-hydroxyphenyl-3-methoxyphenyl)-1-phenylprop-2-en-1-one; toluene-4-sulfonic acid; ozone; acetic acid; triethylamine; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; lithium diisopropyl amide; In tetrahydrofuran; diethyl ether; dichloromethane; N,N-dimethyl-formamide;