dimethylamino[4-(4-propylcyclohexyl)phenyl]methylidene-tetrafluoro(phenyl)phosphorane adduct

Base Information

Chemical Name:dimethylamino[4-(4-propylcyclohexyl)phenyl]methylidene-tetrafluoro(phenyl)phosphorane adduct
CAS No.:1455481-89-6
Molecular Formula:C₂₄H₃₂F₄NP
Molecular Weight:441.492
Hs Code.:

Synonyms:dimethylamino[4-(4-propylcyclohexyl)phenyl]methylidene-tetrafluoro(phenyl)phosphorane adduct

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Chemical Property of dimethylamino[4-(4-propylcyclohexyl)phenyl]methylidene-tetrafluoro(phenyl)phosphorane adduct

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Technology Process of dimethylamino[4-(4-propylcyclohexyl)phenyl]methylidene-tetrafluoro(phenyl)phosphorane adduct

There total 4 articles about dimethylamino[4-(4-propylcyclohexyl)phenyl]methylidene-tetrafluoro(phenyl)phosphorane adduct which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 1455481-76-1
1,1-difluoro-N,N-dimethyl-1-[4-(4-propylcyclohexyl)phenyl]methanamine

: 657-97-6
phenyldifluorophosphine

: 1455481-89-6
dimethylamino[4-(4-propylcyclohexyl)phenyl]methylidene-tetrafluoro(phenyl)phosphorane adduct

Guidance literature:: In diethyl ether; at -40 - 20 ℃; Inert atmosphere;
DOI:10.1016/j.tet.2013.07.062

Reference yield:

: trans-4-(4-n-propylcyclohexyl)benzoic acid

: 1455481-89-6
dimethylamino[4-(4-propylcyclohexyl)phenyl]methylidene-tetrafluoro(phenyl)phosphorane adduct

Guidance literature:: Multi-step reaction with 4 steps

1.1: thionyl chloride / Inert atmosphere; Reflux

2.1: Inert atmosphere

3.1: oxalyl dichloride / dichloromethane / Inert atmosphere; Reflux

3.2: 3 h / 20 °C / Inert atmosphere

4.1: diethyl ether / -40 - 20 °C / Inert atmosphere

With thionyl chloride; oxalyl dichloride; In diethyl ether; dichloromethane;
DOI:10.1016/j.tet.2013.07.062

Reference yield:

: 82492-58-8
4-(trans-4'-propylcyclohexyl) benzoic acid chloride

: 1455481-89-6
dimethylamino[4-(4-propylcyclohexyl)phenyl]methylidene-tetrafluoro(phenyl)phosphorane adduct

Guidance literature:: Multi-step reaction with 3 steps

1.1: Inert atmosphere

2.1: oxalyl dichloride / dichloromethane / Inert atmosphere; Reflux

2.2: 3 h / 20 °C / Inert atmosphere

3.1: diethyl ether / -40 - 20 °C / Inert atmosphere

With oxalyl dichloride; In diethyl ether; dichloromethane;
DOI:10.1016/j.tet.2013.07.062