4,4'-((2-fluoro-1,4-phenylene)bis(ethyne-2,1-diyl))bis(2-chloro-1-methoxybenzene)

Base Information

Chemical Name:4,4'-((2-fluoro-1,4-phenylene)bis(ethyne-2,1-diyl))bis(2-chloro-1-methoxybenzene)
CAS No.:1379597-70-2
Molecular Formula:C₂₄H₁₅Cl₂FO₂
Molecular Weight:425.286
Hs Code.:

Synonyms:4,4'-((2-fluoro-1,4-phenylene)bis(ethyne-2,1-diyl))bis(2-chloro-1-methoxybenzene)

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Chemical Property of 4,4'-((2-fluoro-1,4-phenylene)bis(ethyne-2,1-diyl))bis(2-chloro-1-methoxybenzene)

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Technology Process of 4,4'-((2-fluoro-1,4-phenylene)bis(ethyne-2,1-diyl))bis(2-chloro-1-methoxybenzene)

There total 2 articles about 4,4'-((2-fluoro-1,4-phenylene)bis(ethyne-2,1-diyl))bis(2-chloro-1-methoxybenzene) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 75676-72-1
2-chloro-4-iodo-1-methoxybenzene

: 137000-66-9
1,4-diethynyl-2-fluorobenzene

: 1379597-70-2
4,4'-((2-fluoro-1,4-phenylene)bis(ethyne-2,1-diyl))bis(2-chloro-1-methoxybenzene)

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine; In tetrahydrofuran; at 45 ℃; for 21h; Inert atmosphere;
DOI:10.1021/jo300746x

Reference yield: 43.0%

: 75676-72-1
2-chloro-4-iodo-1-methoxybenzene

: 1435-52-5
2,5-dibromofluorobenzene

: 471-25-0
Propiolic acid

: 1379597-70-2
4,4'-((2-fluoro-1,4-phenylene)bis(ethyne-2,1-diyl))bis(2-chloro-1-methoxybenzene)

Guidance literature:: 2,5-dibromofluorobenzene; Propiolic acid; With bis-triphenylphosphine-palladium(II) chloride; 1,1'-bis-(diphenylphosphino)ferrocene; 1,8-diazabicyclo[5.4.0]undec-7-ene; In dimethyl sulfoxide; at 50 ℃; for 21h; Inert atmosphere;

2-chloro-4-iodo-1-methoxybenzene; In dimethyl sulfoxide; at 50 - 80 ℃; for 7h; Inert atmosphere;
DOI:10.1021/jo300746x

Reference yield: 99.0%

: 1379597-70-2
4,4'-((2-fluoro-1,4-phenylene)bis(ethyne-2,1-diyl))bis(2-chloro-1-methoxybenzene)

: 1379597-72-4
(E,E)-1-fluoro-2,5-bis(3-chloro-4-methoxy-1,1',2,2'-tetradeuterostyryl)benzene

Guidance literature:: With bis(η3-allyl-μ-chloropalladium(II)); 1,1,1,2,2,2-hexamethyldisilane; water-d2; triphenylphosphine; In N,N-dimethyl acetamide; at 80 ℃; for 15h; Inert atmosphere;
DOI:10.1021/jo300746x