C₃₃H₄₇NO₃S₂

Base Information

Chemical Name:C₃₃H₄₇NO₃S₂
CAS No.:1351657-12-9
Molecular Formula:C₃₃H₄₇NO₃S₂
Molecular Weight:569.873
Hs Code.:

C<sub>33</sub>H<sub>47</sub>NO<sub>3</sub>S<sub>2</sub>

Synonyms:C₃₃H₄₇NO₃S₂

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Chemical Property of C₃₃H₄₇NO₃S₂

Chemical Property:

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Technology Process of C₃₃H₄₇NO₃S₂

There total 23 articles about C₃₃H₄₇NO₃S₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 1351657-11-8
C₂₆H₄₄O₄

: 149-30-4,118090-09-8
2-Mercaptobenzothiazole

: 1351657-12-9
C₃₃H₄₇NO₃S₂

Guidance literature:: With di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran;
DOI:10.1016/j.tetlet.2011.10.073

Reference yield:

: 80657-88-1
(2R,4R)-2-Methyl-4-((4S,5R)-2,2,5-trimethyl-[1,3]dioxan-4-yl)-pentan-1-ol

: 1351657-12-9
C₃₃H₄₇NO₃S₂

Guidance literature:: Multi-step reaction with 18 steps

1: oxalyl dichloride; dimethyl sulfoxide; triethylamine / dichloromethane

2: sodium hydride / tetrahydrofuran

3: diisobutylaluminium hydride / tetrahydrofuran

4: titanium(IV) isopropylate; tert.-butylhydroperoxide; diethyl (2S,3S)-tartrate / dichloromethane

5: pyridine; tributylphosphine

6: dichloromethane

7: tetra-(n-butyl)ammonium iodide; sodium hydride / N,N-dimethyl-formamide

8: sodium periodate / methanol; water

9: 2,6-dimethylpyridine; trifluoroacetic anhydride / acetonitrile

10: sodium hydride / tetrahydrofuran

11: aluminum oxide; 20 % Pd(OH)2/C; hydrogen / ethanol

12: pyridinium p-toluenesulfonate / 1,2-dichloro-ethane

13: lithium diisopropyl amide / tetrahydrofuran

14: lithium aluminium tetrahydride / tetrahydrofuran

15: 1H-imidazole / dichloromethane

16: tetra-(n-butyl)ammonium iodide; potassium hydride / tetrahydrofuran

17: tetrabutyl ammonium fluoride / tetrahydrofuran

18: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran

With pyridine; 1H-imidazole; 2,6-dimethylpyridine; titanium(IV) isopropylate; tert.-butylhydroperoxide; aluminum oxide; sodium periodate; lithium aluminium tetrahydride; oxalyl dichloride; diethyl (2S,3S)-tartrate; tributylphosphine; di-isopropyl azodicarboxylate; 20 % Pd(OH)2/C; tetrabutyl ammonium fluoride; hydrogen; pyridinium p-toluenesulfonate; tetra-(n-butyl)ammonium iodide; potassium hydride; sodium hydride; diisobutylaluminium hydride; dimethyl sulfoxide; triethylamine; triphenylphosphine; trifluoroacetic anhydride; lithium diisopropyl amide; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; 1,2-dichloro-ethane; N,N-dimethyl-formamide; acetonitrile; 1: Swern oxidation / 2: Horner-Emmons olefination / 4: Katsuki-Sharpless epoxidation / 9: Pummerer rearrangement / 10: Horner-Emmons olefination;
DOI:10.1016/j.tetlet.2011.10.073

Reference yield:

: 1351656-96-6
C₁₄H₂₆O₄

: 1351657-12-9
C₃₃H₄₇NO₃S₂

Guidance literature:: Multi-step reaction with 19 steps

1: diisobutylaluminium hydride / tetrahydrofuran

2: oxalyl dichloride; dimethyl sulfoxide; triethylamine / dichloromethane

3: sodium hydride / tetrahydrofuran

4: diisobutylaluminium hydride / tetrahydrofuran

5: titanium(IV) isopropylate; tert.-butylhydroperoxide; diethyl (2S,3S)-tartrate / dichloromethane

6: pyridine; tributylphosphine

7: dichloromethane

8: tetra-(n-butyl)ammonium iodide; sodium hydride / N,N-dimethyl-formamide

9: sodium periodate / methanol; water

10: 2,6-dimethylpyridine; trifluoroacetic anhydride / acetonitrile

11: sodium hydride / tetrahydrofuran

12: aluminum oxide; 20 % Pd(OH)2/C; hydrogen / ethanol

13: pyridinium p-toluenesulfonate / 1,2-dichloro-ethane

14: lithium diisopropyl amide / tetrahydrofuran

15: lithium aluminium tetrahydride / tetrahydrofuran

16: 1H-imidazole / dichloromethane

17: tetra-(n-butyl)ammonium iodide; potassium hydride / tetrahydrofuran

18: tetrabutyl ammonium fluoride / tetrahydrofuran

19: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran

With pyridine; 1H-imidazole; 2,6-dimethylpyridine; titanium(IV) isopropylate; tert.-butylhydroperoxide; aluminum oxide; sodium periodate; lithium aluminium tetrahydride; oxalyl dichloride; diethyl (2S,3S)-tartrate; tributylphosphine; di-isopropyl azodicarboxylate; 20 % Pd(OH)2/C; tetrabutyl ammonium fluoride; hydrogen; pyridinium p-toluenesulfonate; tetra-(n-butyl)ammonium iodide; potassium hydride; sodium hydride; diisobutylaluminium hydride; dimethyl sulfoxide; triethylamine; triphenylphosphine; trifluoroacetic anhydride; lithium diisopropyl amide; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; 1,2-dichloro-ethane; N,N-dimethyl-formamide; acetonitrile; 2: Swern oxidation / 3: Horner-Emmons olefination / 5: Katsuki-Sharpless epoxidation / 10: Pummerer rearrangement / 11: Horner-Emmons olefination;
DOI:10.1016/j.tetlet.2011.10.073