C₂₆H₃₂N₂O₃

Base Information

Chemical Name:C₂₆H₃₂N₂O₃
CAS No.:1416772-62-7
Molecular Formula:C₂₆H₃₂N₂O₃
Molecular Weight:420.552
Hs Code.:

C<sub>26</sub>H<sub>32</sub>N<sub>2</sub>O<sub>3</sub>

Synonyms:C₂₆H₃₂N₂O₃

Suppliers and Price of C₂₆H₃₂N₂O₃

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₂₆H₃₂N₂O₃

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₂₆H₃₂N₂O₃

There total 9 articles about C₂₆H₃₂N₂O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 1416772-52-5
C₂₆H₃₀N₂O

: 1416772-62-7
C₂₆H₃₂N₂O₃

Guidance literature:: With methanesulfonamide; AD-mix-α; In water; tert-butyl alcohol; at 20 ℃; for 72h; Inert atmosphere; Schlenk technique;
DOI:10.1021/ml300385q

Reference yield:

: 89890-92-6
N-acetyl-(β-3-pyridyl)-α,β-dehydroalanine

: 1416772-62-7
C₂₆H₃₂N₂O₃

Guidance literature:: Multi-step reaction with 8 steps

1.1: sodium acetate / 72 h / 20 °C / Inert atmosphere; Schlenk technique

2.1: tetrafluoroboric acid; (R,R)-(-)-1,2-bis[(o-methoxyphenyl)(phenyl) phosphino]ethane(1,5-cyclooctadiene)rhodium(I) tetrafluoroborate; hydrogen / methanol / 18 h / 50 °C / 3750.38 Torr / Autoclave; Schlenk technique

3.1: thionyl chloride / methanol / 18 h / 0 - 80 °C / Inert atmosphere; Schlenk technique

4.1: sodium cyanoborohydride; acetic acid / methanol / 24 h / 20 °C / Molecular sieve; Inert atmosphere; Schlenk technique

5.1: lithium aluminium tetrahydride / diethyl ether / 0.5 h / 0 °C / Inert atmosphere; Schlenk technique

6.1: Dess-Martin periodane / dichloromethane / 0.5 h / 0 °C / Inert atmosphere; Schlenk technique

7.1: chromium dichloride / tetrahydrofuran / 0.42 h / 200 °C / Inert atmosphere; Schlenk technique

7.2: 3 h / 20 °C

8.1: AD-mix-α; methanesulfonamide / water; tert-butyl alcohol / 72 h / 20 °C / Inert atmosphere; Schlenk technique

With chromium dichloride; lithium aluminium tetrahydride; tetrafluoroboric acid; thionyl chloride; (R,R)-(-)-1,2-bis[(o-methoxyphenyl)(phenyl) phosphino]ethane(1,5-cyclooctadiene)rhodium(I) tetrafluoroborate; methanesulfonamide; AD-mix-α; hydrogen; sodium acetate; sodium cyanoborohydride; Dess-Martin periodane; acetic acid; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; water; tert-butyl alcohol;
DOI:10.1021/ml300385q

Reference yield:

: 115167-43-6
methyl (Z)-2-acetamido-3-(3-pyridyl)propenoate

: 1416772-62-7
C₂₆H₃₂N₂O₃

Guidance literature:: Multi-step reaction with 7 steps

1.1: tetrafluoroboric acid; (R,R)-(-)-1,2-bis[(o-methoxyphenyl)(phenyl) phosphino]ethane(1,5-cyclooctadiene)rhodium(I) tetrafluoroborate; hydrogen / methanol / 18 h / 50 °C / 3750.38 Torr / Autoclave; Schlenk technique

2.1: thionyl chloride / methanol / 18 h / 0 - 80 °C / Inert atmosphere; Schlenk technique

3.1: sodium cyanoborohydride; acetic acid / methanol / 24 h / 20 °C / Molecular sieve; Inert atmosphere; Schlenk technique

4.1: lithium aluminium tetrahydride / diethyl ether / 0.5 h / 0 °C / Inert atmosphere; Schlenk technique

5.1: Dess-Martin periodane / dichloromethane / 0.5 h / 0 °C / Inert atmosphere; Schlenk technique

6.1: chromium dichloride / tetrahydrofuran / 0.42 h / 200 °C / Inert atmosphere; Schlenk technique

6.2: 3 h / 20 °C

7.1: AD-mix-α; methanesulfonamide / water; tert-butyl alcohol / 72 h / 20 °C / Inert atmosphere; Schlenk technique

With chromium dichloride; lithium aluminium tetrahydride; tetrafluoroboric acid; thionyl chloride; (R,R)-(-)-1,2-bis[(o-methoxyphenyl)(phenyl) phosphino]ethane(1,5-cyclooctadiene)rhodium(I) tetrafluoroborate; methanesulfonamide; AD-mix-α; hydrogen; sodium cyanoborohydride; Dess-Martin periodane; acetic acid; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; water; tert-butyl alcohol;
DOI:10.1021/ml300385q