dithiocarbonic acid O-ethyl ester S-(2-isothiocyanato-5-methyl-benzyl) ester

Base Information

Chemical Name:dithiocarbonic acid O-ethyl ester S-(2-isothiocyanato-5-methyl-benzyl) ester
CAS No.:655230-84-5
Molecular Formula:C₁₂H₁₃NOS₃
Molecular Weight:283.439
Hs Code.:

dithiocarbonic acid <i>O</i>-ethyl ester <i>S</i>-(2-isothiocyanato-5-methyl-benzyl) ester

Synonyms:dithiocarbonic acid O-ethyl ester S-(2-isothiocyanato-5-methyl-benzyl) ester

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Chemical Property of dithiocarbonic acid O-ethyl ester S-(2-isothiocyanato-5-methyl-benzyl) ester

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Technology Process of dithiocarbonic acid O-ethyl ester S-(2-isothiocyanato-5-methyl-benzyl) ester

There total 3 articles about dithiocarbonic acid O-ethyl ester S-(2-isothiocyanato-5-methyl-benzyl) ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 75-15-0,12122-00-8
carbon disulfide

: 655230-20-9
dithiocarbonic acid O-ethyl ester S-(5-methyl-2-triphenylphosphoranylideneamino)benzyl ester

: 655230-84-5
dithiocarbonic acid O-ethyl ester S-(2-isothiocyanato-5-methyl-benzyl) ester

Guidance literature:: In benzene; for 12h; Heating;
DOI:10.1039/b310593h

Reference yield:

: 146954-08-7
2-azido-5-methylbenzyl chloride

: 655230-84-5
dithiocarbonic acid O-ethyl ester S-(2-isothiocyanato-5-methyl-benzyl) ester

Guidance literature:: Multi-step reaction with 3 steps

1: 88 percent / acetone / 1 h / 20 °C

2: 75 percent / diethyl ether / 6 h / 20 °C

3: 98 percent / benzene / 12 h / Heating

In diethyl ether; acetone; benzene;
DOI:10.1039/b310593h

Reference yield:

: 655230-01-6
dithiocarbonic acid O-ethyl ester S-(2-azido-5-methylbenzyl) ester

: 655230-84-5
dithiocarbonic acid O-ethyl ester S-(2-isothiocyanato-5-methyl-benzyl) ester

Guidance literature:: Multi-step reaction with 2 steps

1: 75 percent / diethyl ether / 6 h / 20 °C

2: 98 percent / benzene / 12 h / Heating

In diethyl ether; benzene;
DOI:10.1039/b310593h