C₃₀H₅₄O₇Si

Base Information

Chemical Name:C₃₀H₅₄O₇Si
CAS No.:1609652-08-5
Molecular Formula:C₃₀H₅₄O₇Si
Molecular Weight:554.84
Hs Code.:

C<sub>30</sub>H<sub>54</sub>O<sub>7</sub>Si

Synonyms:C₃₀H₅₄O₇Si

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Chemical Property of C₃₀H₅₄O₇Si

Chemical Property:

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Technology Process of C₃₀H₅₄O₇Si

There total 19 articles about C₃₀H₅₄O₇Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1609652-07-4
C₄₀H₆₃NO₈Si

: 1609652-08-5
C₃₀H₅₄O₇Si

Guidance literature:: With lithium hydroxide monohydrate; dihydrogen peroxide; In tetrahydrofuran; water; at 0 ℃; for 5h;
DOI:10.1039/c4ob00323c

Reference yield:

: 132015-83-9
((4S,5R)-2,2-dimethyl-5-propyl-1,3-dioxolan-4-yl)methanol

: 1609652-08-5
C₃₀H₅₄O₇Si

Guidance literature:: Multi-step reaction with 18 steps

1.1: dmap; triethylamine / dichloromethane / 0 - 20 °C

2.1: toluene-4-sulfonic acid / methanol / 0 - 20 °C

3.1: potassium carbonate / methanol / 2 h / 0 °C

4.1: sodium hydride / tetrahydrofuran; mineral oil / 1 h / 0 °C

4.2: 0 - 20 °C

5.1: copper(I) bromide / tetrahydrofuran; diethyl ether / 0 °C

6.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 8 h / 0 - 20 °C

7.1: ozone / dichloromethane / -78 °C / Inert atmosphere

8.1: benzene / 2 h / 20 °C

9.1: diisobutylaluminium hydride / dichloromethane; toluene / 20 °C / Cooling

10.1: titanium(IV) isopropylate; D-(-)-diisopropyl tartrate / dichloromethane / 0.5 h / -20 °C / Molecular sieve

10.2: 3 h / -20 °C

11.1: sodium bis(2-methoxyethoxy)aluminium dihydride / tetrahydrofuran; toluene / 2.5 h / 0 °C

12.1: pyridinium p-toluenesulfonate / dichloromethane / 0 °C

13.1: diisobutylaluminium hydride / dichloromethane; toluene / 2 h / -20 °C

14.1: Dess-Martin periodane / dichloromethane / 1 h / 0 - 20 °C

15.1: titanium tetrachloride / dichloromethane / 0.08 h / 0 °C

15.2: 0.5 h

15.3: 1 h / -78 - 0 °C

16.1: 2,6-dimethylpyridine / dichloromethane / 2 h / -78 °C

17.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 0 °C / pH 7

18.1: lithium hydroxide monohydrate; dihydrogen peroxide / tetrahydrofuran; water / 5 h / 0 °C

With 2,6-dimethylpyridine; titanium(IV) isopropylate; dmap; lithium hydroxide monohydrate; dihydrogen peroxide; pyridinium p-toluenesulfonate; titanium tetrachloride; sodium hydride; diisobutylaluminium hydride; potassium carbonate; D-(-)-diisopropyl tartrate; Dess-Martin periodane; toluene-4-sulfonic acid; ozone; triethylamine; N-ethyl-N,N-diisopropylamine; sodium bis(2-methoxyethoxy)aluminium dihydride; 2,3-dicyano-5,6-dichloro-p-benzoquinone; copper(I) bromide; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; water; toluene; mineral oil; benzene; 8.1: |Wittig Olefination / 10.1: |Sharpless Asymmetric Epoxidation / 15.2: |Evans Aldol Reaction;
DOI:10.1039/c4ob00323c

Reference yield:

: 1609652-00-7
(3R,6S,7R)-7-((4-methoxybenzyl)oxy)-6-(methoxymethoxy)dodecane-1,3-diol

: 1609652-08-5
C₃₀H₅₄O₇Si

Guidance literature:: Multi-step reaction with 7 steps

1.1: pyridinium p-toluenesulfonate / dichloromethane / 0 °C

2.1: diisobutylaluminium hydride / dichloromethane; toluene / 2 h / -20 °C

3.1: Dess-Martin periodane / dichloromethane / 1 h / 0 - 20 °C

4.1: titanium tetrachloride / dichloromethane / 0.08 h / 0 °C

4.2: 0.5 h

4.3: 1 h / -78 - 0 °C

5.1: 2,6-dimethylpyridine / dichloromethane / 2 h / -78 °C

6.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 0 °C / pH 7

7.1: lithium hydroxide monohydrate; dihydrogen peroxide / tetrahydrofuran; water / 5 h / 0 °C

With 2,6-dimethylpyridine; lithium hydroxide monohydrate; dihydrogen peroxide; pyridinium p-toluenesulfonate; titanium tetrachloride; diisobutylaluminium hydride; Dess-Martin periodane; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In tetrahydrofuran; dichloromethane; water; toluene; 4.2: |Evans Aldol Reaction;
DOI:10.1039/c4ob00323c