N²-<2-Benzoyl-vinyl>-α-amino-essigsaeure-benzylamid

Base Information

• Chemical Name: N²-<2-Benzoyl-vinyl>-α-amino-essigsaeure-benzylamid
• CAS No.: 17038-68-5
• Molecular Formula: C₁₈H₁₈N₂O₂
• Molecular Weight: 294.353
• Mol file: 17038-68-5.mol

Synonyms:N²-<2-Benzoyl-vinyl>-α-amino-essigsaeure-benzylamid

Chemical Property of N²-<2-Benzoyl-vinyl>-α-amino-essigsaeure-benzylamid

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N²-<2-Benzoyl-vinyl>-α-amino-essigsaeure-benzylamid

There total 3 articles about N²-<2-Benzoyl-vinyl>-α-amino-essigsaeure-benzylamid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-Oxo-3-phenylpropanal (15397-33-8) → N2-<2-Benzoyl-vinyl>-α-amino-essigsaeure-benzylamid (17038-68-5)

Guidance literature:

Multi-step reaction with 2 steps

2: (i) Et₂Mg, Et₂O, dioxane, (ii) /BRN= 2583613/, (iii) benzene

DOI:10.1016/S0040-4039(01)89754-9

Reference yield:

Ethyl N-(3-oxo-3-phenylprop-1-enyl)glycinate (13945-24-9) + benzylamine (100-46-9) → N2-<2-Benzoyl-vinyl>-α-amino-essigsaeure-benzylamid (17038-68-5)

Guidance literature:

Multistep reaction; (i) Et₂Mg, Et₂O, dioxane, (ii) /BRN= 2583613/, benzene, (iii) Na₂H₂edta, H₂O;

DOI:10.1039/j39680001704

Reference yield:

Bis-<1-phenyl-propandion-(1,3)>-Cu(II)-chelat → N2-<2-Benzoyl-vinyl>-α-amino-essigsaeure-benzylamid (17038-68-5)

Guidance literature:

Multi-step reaction with 2 steps

1: (i) aq. HCl, CHCl₃, (ii) /BRN= 3594034/

2: (i) Et₂Mg, Et₂O, dioxane, (ii) /BRN= 2583613/, benzene, (iii) Na₂H₂edta, H₂O

DOI:10.1039/j39680001704

upstream raw materials:

Ethyl N-(3-oxo-3-phenylprop-1-enyl)glycinate

benzylamine

3-Oxo-3-phenylpropanal

Downstream raw materials:

N-benzyl-2-aminoacetamide

N-(2-Hydroxy-naphthyl-⁽¹⁾-methylen)-glycin-(N-benzyl-amid)