C₂₄H₄₅N₅O₅

Base Information

• Chemical Name: C₂₄H₄₅N₅O₅
• CAS No.: 1375968-67-4
• Molecular Formula: C₂₄H₄₅N₅O₅
• Molecular Weight: 483.652

Synonyms:C₂₄H₄₅N₅O₅

Chemical Property of C₂₄H₄₅N₅O₅

Chemical Property:

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Technology Process of C₂₄H₄₅N₅O₅

There total 1 articles about C₂₄H₄₅N₅O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

tert-butyl (3S)-3-aminopiperidine-1-carboxylate (625471-18-3) → C24H45N5O5 (1375968-67-4)

Guidance literature:

Multi-step reaction with 9 steps

1.1: sodium sulfate / dichloromethane; toluene / 2 h / 20 °C

1.2: 1.5 h / 20 °C

2.1: sodium tris(acetoxy)borohydride; acetic acid / dichloromethane; toluene / 1.5 h / 20 °C

3.1: triethylamine / dichloromethane / 17 h / 0 - 20 °C

4.1: trifluoroacetic acid / dichloromethane / 16 h / 20 °C

5.1: benzotriazol-1-ol; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide / dichloromethane / 0.25 h / 0 °C / Molecular sieve

5.2: 15 h / 20 °C

6.1: trifluoroacetic acid / dichloromethane / 16 h / 20 °C

7.1: benzotriazol-1-ol; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide / dichloromethane / 0.25 h / 0 °C / Molecular sieve

7.2: 15 h / 20 °C

8.1: ammonia / methanol / 119 h / 20 °C

9.1: palladium 10% on activated carbon; hydrogen / 144 h / 20 °C

With palladium 10% on activated carbon; ammonia; hydrogen; sodium tris(acetoxy)borohydride; benzotriazol-1-ol; acetic acid; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; sodium sulfate; triethylamine; trifluoroacetic acid; In methanol; dichloromethane; toluene;

DOI:10.1021/jm201517a

upstream raw materials:

tert-butyl (3S)-3-aminopiperidine-1-carboxylate

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