Benzeneethanamine, 2-amino-N-methyl- (9CI)

Base Information

• Chemical Name: Benzeneethanamine, 2-amino-N-methyl- (9CI)
• CAS No.: 22908-49-2
• Molecular Formula: C9H14 N2
• Molecular Weight: 150.224
• Hs Code.: 2921590090
• Mol file: 22908-49-2.mol

Synonyms:Phenethylamine,o-amino-N-methyl- (7CI,8CI); 2-(2-Methylaminoethyl)phenylamine

Chemical Property of Benzeneethanamine, 2-amino-N-methyl- (9CI)

Chemical Property:

• PSA: 38.05000
• LogP: 2.00280

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Benzeneethanamine, 2-amino-N-methyl- (9CI)

There total 2 articles about Benzeneethanamine, 2-amino-N-methyl- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

methyl-(2-nitro-phenethyl)-amine (33100-16-2) → 2-(2-methylamino-ethyl)-phenylamine (22908-49-2)

Guidance literature:

With hydrogen; Raney nickel; In ethanol; at 20 ℃; for 2h; under 3102.97 Torr;

Reference yield:

→ 2-(2-methylamino-ethyl)-phenylamine (22908-49-2)

Guidance literature:

N-Methyl-o-amino-phenylacetamid, LiAlH4, 1,2-Dimethoxy-ethan, Siedetemp.;

DOI:10.1039/jr9630004924

Reference yield: 44.0%

di-tert-butyl dicarbonate (24424-99-5) + 2-(2-methylamino-ethyl)-phenylamine (22908-49-2) → N-(2-(2-amino-phenyl)ethyl)-N-methylcarbamic acid tert-butyl ester (202811-15-2) + N-{2-[2-(N-(tert-butoxycarbonyl)-N-methylamino)ethyl]-phenyl}carbamic acid tert-butyl ester

Guidance literature:

With sodium hydroxide; In tetrahydrofuran; at 20 ℃; for 16h;

DOI:10.1016/S0223-5234(00)00160-4

upstream raw materials:

methyl-(2-nitro-phenethyl)-amine

Downstream raw materials:

N-(2-(2-amino-phenyl)ethyl)-N-methylcarbamic acid tert-butyl ester

N-(2-(2-(methylamino)-ethyl)phenyl)methanesulfonamide

N-[2-(2-(methylamino)ethyl)phenyl]benzenesulfonamide

N-(2-(2-(methylsulfonylamino)phenyl)ethyl)-N-methylcarbamic acid tert-butyl ester

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