9-Anthracenemethanamine

Base Information

• Chemical Name: 9-Anthracenemethanamine
• CAS No.: 2476-68-8
• Molecular Formula: C15H13 N
• Molecular Weight: 207.275
• Hs Code.: 2921499090
• DSSTox Substance ID: DTXSID20454662
• Nikkaji Number: J903.648B
• Wikidata: Q82276321
• ChEMBL ID: CHEMBL46449
• Mol file: 2476-68-8.mol

Synonyms:9-Anthracenemethanamine;Anthracen-9-ylmethanamine;2476-68-8;C-Anthracen-9-yl-methylamine;anthracen-10-ylmethanamine;CHEMBL46449;9-aminomethylanthracene;Anthracene-9-methanamine;SCHEMBL2384515;DTXSID20454662;BDBM50111529;SB77878;BS-48901;CS-0187882;N14949

Chemical Property of 9-Anthracenemethanamine

Chemical Property:

• Melting Point: 38-40 °C
• Boiling Point: 405.8±14.0 °C(Predicted)
• PKA: 9.06±0.30(Predicted)
• PSA: 26.02000
• Density: 1.166±0.06 g/cm3(Predicted)
• LogP: 4.15200
• XLogP3: 3.6
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 1
• Exact Mass: 207.104799419
• Heavy Atom Count: 16
• Complexity: 216

Purity/Quality:

98.5% ^*data from raw suppliers

C-Anthracen-9-yl-methylamine 95 ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC=C2C(=C1)C=C3C=CC=CC3=C2CN

Technology Process of 9-Anthracenemethanamine

There total 13 articles about 9-Anthracenemethanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

9-(azidomethyl)anthracene (195133-98-3) → 9-(aminomethyl)anthracene (2476-68-8)

Guidance literature:

With palladium 10% on activated carbon; hydrogen; In ethyl acetate; for 4h; Inert atmosphere;

DOI:10.1016/j.dyepig.2012.01.004

Reference yield: 93.0%

9-bromoethylanthracene (2417-77-8) → 9-(aminomethyl)anthracene (2476-68-8)

Guidance literature:

9-bromoethylanthracene; With hexamethylenetetramine; In chloroform; for 5h; Heating;

With hydrogenchloride; In ethanol; at 70 ℃;

DOI:10.1039/b404706k

Reference yield: 80.0%

N-(9-anthranylmethyl)phthalimide (94617-21-7) → 9-(aminomethyl)anthracene (2476-68-8)

Guidance literature:

With hydrazine hydrate; In tetrahydrofuran; ethanol; for 3h; Ambient temperature;

DOI:10.1021/jm980440p

upstream raw materials:

anthracenylmethyl chloride

9-cyanoanthracene

9-(azidomethyl)anthracene

N-(9-anthranylmethyl)phthalimide

Downstream raw materials:

C₄₇H₄₁N₃O₂

9-Anthracene carboxamide

(E)‐anthracene‐9‐carbaldehyde oxime