N-{(7S,8aS)-2-[2-(tert-butylamino)-2-oxoethyl]octahydropyrrolo[1,2-a]-pyrazin-7-yl}-3,4-dichlorobenzamide

Base Information

Chemical Name:N-{(7S,8aS)-2-[2-(tert-butylamino)-2-oxoethyl]octahydropyrrolo[1,2-a]-pyrazin-7-yl}-3,4-dichlorobenzamide
CAS No.:1429294-71-2
Molecular Formula:C₂₀H₂₈Cl₂N₄O₂
Molecular Weight:427.374
Hs Code.:

Synonyms:N-{(7S,8aS)-2-[2-(tert-butylamino)-2-oxoethyl]octahydropyrrolo[1,2-a]-pyrazin-7-yl}-3,4-dichlorobenzamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-{(7S,8aS)-2-[2-(tert-butylamino)-2-oxoethyl]octahydropyrrolo[1,2-a]-pyrazin-7-yl}-3,4-dichlorobenzamide

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Technology Process of N-{(7S,8aS)-2-[2-(tert-butylamino)-2-oxoethyl]octahydropyrrolo[1,2-a]-pyrazin-7-yl}-3,4-dichlorobenzamide

There total 2 articles about N-{(7S,8aS)-2-[2-(tert-butylamino)-2-oxoethyl]octahydropyrrolo[1,2-a]-pyrazin-7-yl}-3,4-dichlorobenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 15678-99-6
N-tert-butylchloroacetamide

: C₁₄H₁₇Cl₂N₃O

: 1429294-71-2
N-{(7S,8aS)-2-[2-(tert-butylamino)-2-oxoethyl]octahydropyrrolo[1,2-a]-pyrazin-7-yl}-3,4-dichlorobenzamide

Guidance literature:: With triethylamine; In dichloromethane; N,N-dimethyl-formamide; at 20 ℃; for 72h;

Reference yield:

: 1429296-96-7
(7S,8aS)-tert-butyl 7-(3,4-dichlorobenzamido)hexahydropyrrolo[1,2-a]-pyrazine-2(1H)-carboxylate

: 1429294-71-2
N-{(7S,8aS)-2-[2-(tert-butylamino)-2-oxoethyl]octahydropyrrolo[1,2-a]-pyrazin-7-yl}-3,4-dichlorobenzamide

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride / dichloromethane; 1,4-dioxane; water; methanol / 3 h / 20 °C

2: triethylamine / dichloromethane; N,N-dimethyl-formamide / 72 h / 20 °C

With hydrogenchloride; triethylamine; In 1,4-dioxane; methanol; dichloromethane; water; N,N-dimethyl-formamide;