dicarbonyl(3-methylpentadienyl)(triphenylphosphine)iron hexafluorophosphate

Base Information

Chemical Name:dicarbonyl(3-methylpentadienyl)(triphenylphosphine)iron hexafluorophosphate
CAS No.:898263-22-4
Molecular Formula:C₂₆H₂₄FeO₂P*F₆P
Molecular Weight:600.26
Hs Code.:

Synonyms:dicarbonyl(3-methylpentadienyl)(triphenylphosphine)iron hexafluorophosphate

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Chemical Property of dicarbonyl(3-methylpentadienyl)(triphenylphosphine)iron hexafluorophosphate

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Technology Process of dicarbonyl(3-methylpentadienyl)(triphenylphosphine)iron hexafluorophosphate

There total 1 articles about dicarbonyl(3-methylpentadienyl)(triphenylphosphine)iron hexafluorophosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: hexafluorophosphoric acid

: dicarbonyl(3-methyl-2,4-pentadien-1-ol)(triphenylphosphine)iron

: 898263-22-4
dicarbonyl(3-methylpentadienyl)(triphenylphosphine)iron hexafluorophosphate

Guidance literature:: In diethyl ether; acetic anhydride; addn. of ice cold soln. of iron compd. and acetic anhydride in ether to ice cold soln. of acetic anhydride and HPF6, stirring for 30 min; addn. to ether, filtration, washing with ether, drying in vac., elem. anal.;
DOI:10.1021/om7006248

Reference yield: 99.0%

: 898263-22-4
dicarbonyl(3-methylpentadienyl)(triphenylphosphine)iron hexafluorophosphate

: 1074-82-4
potassium phtalimide

: Fe(CO)2(CH₂CHC(CH₃)CHCH₂NC₂O₂C₆H₄)(P(C₆H₅)3)

Guidance literature:: In tetrahydrofuran; addn. of phthalimide satl to soln. of iron compd. in THF at 0°C under N2, stirring at room temp. for 30 min; addn. to satd. soln. of NH4Cl and water, extn. (ethyl acetate), washing extracts with water, drying with MgSO4, concg., chromy. (SiO2, hexane-ethyl acetate (10:1)), elem. anal.;
DOI:10.1021/om7006248