Technology Process of C14H17N3O3
There total 6 articles about C14H17N3O3 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
sodium hydride;
In
tetrahydrofuran;
at -10 - 20 ℃;
for 5h;
DOI:10.1055/s-2007-973902
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 75 percent / DMAP; Et3N / CH2Cl2 / 24 h / 20 °C
2: 96 percent / TBAF / tetrahydrofuran / 6 h / 20 °C
3: 96 percent / diphenylphosphoryl azide; DBU / toluene / 6 h / 20 °C
4: 93 percent / NMO; osmium hydroxide / various solvents / 18 h / 0 °C
5: 78 percent / NaH / tetrahydrofuran / 5 h / -10 - 20 °C
With
dmap; N-methyl-2-indolinone; diphenylphosphoranyl azide; tetrabutyl ammonium fluoride; sodium hydride; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine;
In
tetrahydrofuran; dichloromethane; various solvents; toluene;
DOI:10.1055/s-2007-973902
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 93 percent / NMO; osmium hydroxide / various solvents / 18 h / 0 °C
2: 78 percent / NaH / tetrahydrofuran / 5 h / -10 - 20 °C
With
N-methyl-2-indolinone; sodium hydride;
In
tetrahydrofuran; various solvents;
DOI:10.1055/s-2007-973902