Technology Process of C37H28O2
There total 6 articles about C37H28O2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
palladium diacetate; caesium carbonate; tricyclohexylphosphine;
In
1,3,5-trimethyl-benzene;
for 24h;
Inert atmosphere;
DOI:10.1021/ol303327k
- Guidance literature:
-
Multi-step reaction with 6 steps
1: triethylamine / acetonitrile / 2.03 h / 0 - 20 °C
2: caesium carbonate; palladium diacetate; tricyclohexylphosphine / 1,3,5-trimethyl-benzene / 24 h / Inert atmosphere; Reflux
3: triethylamine / acetonitrile / 2.02 h / 0 - 20 °C
4: palladium diacetate; potassium fluoride; dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane / tetrahydrofuran; water / 20 h / 20 °C / Inert atmosphere
5: triethylamine / acetonitrile / 17.03 h / 0 - 20 °C
6: caesium carbonate; palladium diacetate; tricyclohexylphosphine / 1,3,5-trimethyl-benzene / 24 h / Inert atmosphere
With
dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; potassium fluoride; palladium diacetate; caesium carbonate; triethylamine; tricyclohexylphosphine;
In
tetrahydrofuran; water; acetonitrile; 1,3,5-trimethyl-benzene;
4: |Suzuki-Miyaura Coupling;
DOI:10.1021/ol303327k
- Guidance literature:
-
Multi-step reaction with 3 steps
1: palladium diacetate; potassium fluoride; dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane / tetrahydrofuran; water / 20 h / 20 °C / Inert atmosphere
2: triethylamine / acetonitrile / 17.03 h / 0 - 20 °C
3: caesium carbonate; palladium diacetate; tricyclohexylphosphine / 1,3,5-trimethyl-benzene / 24 h / Inert atmosphere
With
dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; potassium fluoride; palladium diacetate; caesium carbonate; triethylamine; tricyclohexylphosphine;
In
tetrahydrofuran; water; acetonitrile; 1,3,5-trimethyl-benzene;
1: |Suzuki-Miyaura Coupling;
DOI:10.1021/ol303327k