C₄₇H₆₅N₃O₁₃

Base Information

Chemical Name:C₄₇H₆₅N₃O₁₃
CAS No.:1369430-91-0
Molecular Formula:C₄₇H₆₅N₃O₁₃
Molecular Weight:880.045
Hs Code.:

C<sub>47</sub>H<sub>65</sub>N<sub>3</sub>O<sub>13</sub>

Synonyms:C₄₇H₆₅N₃O₁₃

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Chemical Property of C₄₇H₆₅N₃O₁₃

Chemical Property:

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Technology Process of C₄₇H₆₅N₃O₁₃

There total 23 articles about C₄₇H₆₅N₃O₁₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 21.0%

: 1369430-76-1
C₄₃H₅₅NO₁₄

: 811-93-8
1,1-dimethylethylenediamine

: 1369430-91-0
C₄₇H₆₅N₃O₁₃

Guidance literature:: C₄₃H₅₅NO₁₄; With 1,1'-carbonyldiimidazole; In chloroform; at 20 ℃; for 1h;

1,1-dimethylethylenediamine; In chloroform; at 20 ℃; for 18h;

Reference yield:

: 1369430-93-2
C₅₂H₇₃N₃O₁₅

: 1369430-91-0
C₄₇H₆₅N₃O₁₃

Guidance literature:: With trifluoroacetic acid; In chloroform; at 20 ℃; for 20.1667h;

Reference yield:

: 618-45-1
3-isopropylhydroxybenzene

: 1369430-91-0
C₄₇H₆₅N₃O₁₃

Guidance literature:: Multi-step reaction with 16 steps

1.1: potassium iodate; iodine / water; acetic acid / 20 h / 20 °C

2.1: potassium carbonate / acetonitrile / 2 h / 20 °C

3.1: n-butyllithium / tetrahydrofuran; hexane / -78 °C / Inert atmosphere

3.2: 0.58 h / -78 °C

4.1: methanesulfonic acid / methanol / 14.5 h / 20 °C

5.1: pyridine; acetic anhydride / dmap / 19 h / 4 - 20 °C

6.1: triethylsilane; boron trifluoride diethyl etherate / chloroform; acetonitrile / 1.5 h / 4 °C / Inert atmosphere

7.1: hydrogen / palladium on activated charcoal / methanol / 2 h / 20 °C

8.1: bromine / acetic acid / 20 °C

9.1: water; triethylamine / methanol / 25 h / 20 - 50 °C

10.1: chloro-trimethyl-silane; triethylamine / N,N-dimethyl-formamide / 1 h / 4 °C / Inert atmosphere

11.1: n-butyllithium / tetrahydrofuran; hexane / 0.25 h / -78 °C / Inert atmosphere

11.2: 1 h / -78 °C

12.1: methanesulfonic acid / methanol / 0.5 h / 20 °C

13.1: pyridine; acetic anhydride / dmap / 30 h / 20 °C

14.1: triethylsilane; boron trifluoride diethyl etherate / chloroform; acetonitrile / 0.5 h / 4 - 20 °C / Inert atmosphere

15.1: triethylamine / palladium diacetate; tris-(o-tolyl)phosphine / acetonitrile / 0.33 h / 120 °C / Microwave irradiation; Inert atmosphere

16.1: 1,1'-carbonyldiimidazole / chloroform / 1 h / 20 °C

16.2: 18 h / 20 °C

With pyridine; triethylsilane; n-butyllithium; chloro-trimethyl-silane; methanesulfonic acid; potassium iodate; boron trifluoride diethyl etherate; water; hydrogen; bromine; iodine; acetic anhydride; potassium carbonate; triethylamine; 1,1'-carbonyldiimidazole; dmap; palladium on activated charcoal; palladium diacetate; tris-(o-tolyl)phosphine; In tetrahydrofuran; methanol; hexane; chloroform; water; acetic acid; N,N-dimethyl-formamide; acetonitrile; 15.1: Heck Reaction;