3-(7-Chloro-1,1-dioxo-1H-1λ6-benzo[d]isothiazol-3-yl)-1-(4-fluoro-benzyl)-4-methoxy-isoquinoline

Base Information

Chemical Name:3-(7-Chloro-1,1-dioxo-1H-1λ6-benzo[d]isothiazol-3-yl)-1-(4-fluoro-benzyl)-4-methoxy-isoquinoline
CAS No.:914672-48-3
Molecular Formula:C₂₄H₁₆ClFN₂O₃S
Molecular Weight:466.92
Hs Code.:

Synonyms:3-(7-Chloro-1,1-dioxo-1H-1λ6-benzo[d]isothiazol-3-yl)-1-(4-fluoro-benzyl)-4-methoxy-isoquinoline

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Chemical Property of 3-(7-Chloro-1,1-dioxo-1H-1λ6-benzo[d]isothiazol-3-yl)-1-(4-fluoro-benzyl)-4-methoxy-isoquinoline

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Technology Process of 3-(7-Chloro-1,1-dioxo-1H-1λ6-benzo[d]isothiazol-3-yl)-1-(4-fluoro-benzyl)-4-methoxy-isoquinoline

There total 4 articles about 3-(7-Chloro-1,1-dioxo-1H-1λ6-benzo[d]isothiazol-3-yl)-1-(4-fluoro-benzyl)-4-methoxy-isoquinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₈H₁₄FNO₃

: 914672-48-3
3-(7-Chloro-1,1-dioxo-1H-1λ6-benzo[d]isothiazol-3-yl)-1-(4-fluoro-benzyl)-4-methoxy-isoquinoline

Guidance literature:: Multi-step reaction with 3 steps

1: diethyl cyanophosphonate; N-ethyl-N,N-diisopropylamine / dichloromethane

2: n-butyllithium / tetrahydrofuran

3: sulfuric acid / ethanol / Reflux

With n-butyllithium; diethyl cyanophosphonate; sulfuric acid; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; ethanol; dichloromethane;
DOI:10.1016/j.bmcl.2008.11.060

Reference yield:

: C₂₀H₁₉FN₂O₃

: 914672-48-3
3-(7-Chloro-1,1-dioxo-1H-1λ6-benzo[d]isothiazol-3-yl)-1-(4-fluoro-benzyl)-4-methoxy-isoquinoline

Guidance literature:: Multi-step reaction with 2 steps

1: n-butyllithium / tetrahydrofuran

2: sulfuric acid / ethanol / Reflux

With n-butyllithium; sulfuric acid; In tetrahydrofuran; ethanol;
DOI:10.1016/j.bmcl.2008.11.060